methyl (S)-1-[1-hydroxy-2-(trityloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

Base Information

Chemical Name:methyl (S)-1-[1-hydroxy-2-(trityloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate
CAS No.:1391908-82-9
Molecular Formula:C₃₄H₂₈N₂O₄
Molecular Weight:528.607
Hs Code.:

Synonyms:methyl (S)-1-[1-hydroxy-2-(trityloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (S)-1-[1-hydroxy-2-(trityloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

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Technology Process of methyl (S)-1-[1-hydroxy-2-(trityloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

There total 3 articles about methyl (S)-1-[1-hydroxy-2-(trityloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1042149-39-2
methyl (S)-1-(1,2-dihydroxyethyl)-9H-pyrido[3,4-b]indole-3-carboxylate

: 76-83-5
trityl chloride

: 1391908-82-9
methyl (S)-1-[1-hydroxy-2-(trityloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 5.33333h;
DOI:10.1002/ejoc.201200235

Reference yield:

: 66154-43-6
methyl (S)-1-(2,2-dimethyl-1,3-dioxolan-4-yl)-9H-pyrido[3,4-b]indole-3-carboxylate

: 1391908-82-9
methyl (S)-1-[1-hydroxy-2-(trityloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / tetrahydrofuran; water / 3 h / 20 °C

2: triethylamine / dichloromethane / 5.33 h / 0 - 20 °C

With hydrogenchloride; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/ejoc.201200235

Reference yield:

: C₂₅H₂₈N₂O₆S

: 1391908-82-9
methyl (S)-1-[1-hydroxy-2-(trityloxy)ethyl]-9H-pyrido[3,4-b]indole-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dimethyl sulfoxide / 8 h / 20 °C

2: hydrogenchloride / tetrahydrofuran; water / 3 h / 20 °C

3: triethylamine / dichloromethane / 5.33 h / 0 - 20 °C

With hydrogenchloride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201200235