3-cyclohexylprop-2-enyl bromide

Base Information

Chemical Name:3-cyclohexylprop-2-enyl bromide
CAS No.:131665-81-1
Molecular Formula:C₉H₁₅Br
Molecular Weight:203.122
Hs Code.:

Synonyms:3-cyclohexylprop-2-enyl bromide

Suppliers and Price of 3-cyclohexylprop-2-enyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(3-bromoprop-1-en-1-yl)cyclohexane
25mg
$ 65.00

Total 1 raw suppliers

Chemical Property of 3-cyclohexylprop-2-enyl bromide

Chemical Property:

Purity/Quality:: (3-bromoprop-1-en-1-yl)cyclohexane ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-cyclohexylprop-2-enyl bromide

There total 6 articles about 3-cyclohexylprop-2-enyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 42134-55-4,114096-03-6,132350-24-4
3-cyclohexyl-2-propen-1-ol

: 131665-81-1
3-cyclohexylprop-2-enyl bromide

Guidance literature:: With phosphorus tribromide; for 4h; Ambient temperature;

Reference yield:

: 695-12-5,25498-06-0
vinylcyclohexane

: 106-95-6
allyl bromide

: 131665-81-1
3-cyclohexylprop-2-enyl bromide

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1039/d0cc01316a

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 131665-81-1
3-cyclohexylprop-2-enyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / toluene / 0 °C

1.2: 20 °C

2.1: diisobutylaluminium hydride / dichloromethane / -78 °C

3.1: phosphorus tribromide / diethyl ether / 0 °C

With phosphorus tribromide; sodium hydride; diisobutylaluminium hydride; In diethyl ether; dichloromethane; toluene; 1.1: |Horner-Wadsworth-Emmons Olefination / 1.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1002/ejoc.201301360