trans-4-(phenyl)cyclohexane-1-carbaldehyde

Base Information

Chemical Name:trans-4-(phenyl)cyclohexane-1-carbaldehyde
CAS No.:37810-46-1
Molecular Formula:C₁₃H₁₆O
Molecular Weight:188.269
Hs Code.:

Synonyms:trans-4-(phenyl)cyclohexane-1-carbaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-4-(phenyl)cyclohexane-1-carbaldehyde

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Technology Process of trans-4-(phenyl)cyclohexane-1-carbaldehyde

There total 13 articles about trans-4-(phenyl)cyclohexane-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 701232-23-7
[4-(methoxymethylidene)cyclohexyl]benzene

: 126781-72-4
cis-4-(phenyl)cyclohexane-1-carbaldehyde

: 37810-46-1
trans-4-(phenyl)cyclohexane-1-carbaldehyde

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jacs.7b09901

Reference yield:

: C₁₃H₁₅BrO

: 37810-46-1
trans-4-(phenyl)cyclohexane-1-carbaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride; In tetrahydrofuran; at 20 - 25 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jacs.8b07776

Reference yield:

: 4894-75-1
1-phenyl-4-cyclohexanone

: 4009-98-7
(methoxymethyl)triphenylphosphonium chloride

: 126781-72-4
cis-4-(phenyl)cyclohexane-1-carbaldehyde

: 37810-46-1
trans-4-(phenyl)cyclohexane-1-carbaldehyde

Guidance literature:: (methoxymethyl)triphenylphosphonium chloride; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; Inert atmosphere;

1-phenyl-4-cyclohexanone; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; at 90 ℃; Overall yield = 73 %; Overall yield = 685 mg; Optical yield = 30 %de; Inert atmosphere;
DOI:10.1021/ja406028c