N-[3-(3-cyanopyrazolo[1.5-a]pyrimidin-7-yl)phenyl]-N-carboxymethylacetamide

Base Information

Chemical Name:N-[3-(3-cyanopyrazolo[1.5-a]pyrimidin-7-yl)phenyl]-N-carboxymethylacetamide
CAS No.:1261160-87-5
Molecular Formula:C₁₇H₁₃N₅O₃
Molecular Weight:335.322
Hs Code.:

Synonyms:N-[3-(3-cyanopyrazolo[1.5-a]pyrimidin-7-yl)phenyl]-N-carboxymethylacetamide

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Chemical Property of N-[3-(3-cyanopyrazolo[1.5-a]pyrimidin-7-yl)phenyl]-N-carboxymethylacetamide

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Technology Process of N-[3-(3-cyanopyrazolo[1.5-a]pyrimidin-7-yl)phenyl]-N-carboxymethylacetamide

There total 4 articles about N-[3-(3-cyanopyrazolo[1.5-a]pyrimidin-7-yl)phenyl]-N-carboxymethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7463-31-2
3-Acetamidoacetophenone

: 1261160-87-5
N-[3-(3-cyanopyrazolo[1.5-a]pyrimidin-7-yl)phenyl]-N-carboxymethylacetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 80 °C

2.1: acetic acid / water / 2 h / 50 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 60 °C / Inert atmosphere

3.2: 6 h / 60 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

With sodium hydride; acetic acid; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1261160-86-4
N-[3-(3-cyanopyrazolo[1,5-a]pyrimidin-7-yl)phenyl]-N-(tert-butyloxy-1-oxoeth-2-yl)acetamide

: 1261160-87-5
N-[3-(3-cyanopyrazolo[1.5-a]pyrimidin-7-yl)phenyl]-N-carboxymethylacetamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 96605-61-7
N-(3-(3-(dimethylamino)acryloyl)phenyl)acetamide

: 1261160-87-5
N-[3-(3-cyanopyrazolo[1.5-a]pyrimidin-7-yl)phenyl]-N-carboxymethylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / water / 2 h / 50 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 60 °C / Inert atmosphere

2.2: 6 h / 60 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C

With sodium hydride; acetic acid; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide; mineral oil;