N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-acetimidic acid methyl ester

Base Information

Chemical Name:N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-acetimidic acid methyl ester
CAS No.:107266-95-5
Molecular Formula:C₁₇H₁₈ClNO₃S
Molecular Weight:351.854
Hs Code.:

Synonyms:N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-acetimidic acid methyl ester

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Chemical Property of N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-acetimidic acid methyl ester

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Technology Process of N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-acetimidic acid methyl ester

There total 2 articles about N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-acetimidic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1445-45-0
Trimethyl orthoacetate

: 107266-89-7
2-Amino-5-chlorobenzyl tolyl sulfone

: 107266-95-5
N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-acetimidic acid methyl ester

Guidance literature:: With toluene-4-sulfonic acid; for 2h; Heating;
DOI:10.1055/s-1986-33421

Reference yield:

: 107266-86-4
(5-Chloro-2-nitrophenyl)methyl 4-tolyl sulfone

: 107266-95-5
N-[4-Chloro-2-(toluene-4-sulfonylmethyl)-phenyl]-acetimidic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / Sn, conc. aq. HCl / methanol / 30 - 40 °C

2: 97 percent / p-toluenesulfonic acid / 2 h / Heating

With hydrogenchloride; tin; toluene-4-sulfonic acid; In methanol;
DOI:10.1055/s-1986-33421