N-methyl-N-(4-chlorobutyl) N'-(4-carboxyallyl)phenyl phosphorodiamidic chloride

Base Information

Chemical Name:N-methyl-N-(4-chlorobutyl) N'-(4-carboxyallyl)phenyl phosphorodiamidic chloride
CAS No.:365431-80-7
Molecular Formula:C₁₅H₂₁Cl₂N₂O₃P
Molecular Weight:379.223
Hs Code.:

Synonyms:N-methyl-N-(4-chlorobutyl) N'-(4-carboxyallyl)phenyl phosphorodiamidic chloride

Suppliers and Price of N-methyl-N-(4-chlorobutyl) N'-(4-carboxyallyl)phenyl phosphorodiamidic chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-methyl-N-(4-chlorobutyl) N'-(4-carboxyallyl)phenyl phosphorodiamidic chloride

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of N-methyl-N-(4-chlorobutyl) N'-(4-carboxyallyl)phenyl phosphorodiamidic chloride

There total 3 articles about N-methyl-N-(4-chlorobutyl) N'-(4-carboxyallyl)phenyl phosphorodiamidic chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 62507-78-2
4-aminobenzoic acid allyl ester

: 365432-22-0
N-methyl-N-(4-chlorobutyl)phosphoramidic dichloride

: 365431-80-7
N-methyl-N-(4-chlorobutyl) N'-(4-carboxyallyl)phenyl phosphorodiamidic chloride

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; for 240h; Heating;
DOI:10.1021/jm060142p

Reference yield:

: 138-84-1
potassium 4-aminobenzoate

: 365431-80-7
N-methyl-N-(4-chlorobutyl) N'-(4-carboxyallyl)phenyl phosphorodiamidic chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / dimethylformamide

2: 20 percent / diisopropylethylamine / 1,2-dichloro-ethane / 240 h / Heating

With N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm060142p

Reference yield:

: N-methyl-N-(4-chloro-n-butyl)amine hydrochloride

: 365431-80-7
N-methyl-N-(4-chlorobutyl) N'-(4-carboxyallyl)phenyl phosphorodiamidic chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / POCl₃; Et₃N / CH₂Cl₂ / 20 °C

2: 20 percent / diisopropylethylamine / 1,2-dichloro-ethane / 240 h / Heating

With triethylamine; N-ethyl-N,N-diisopropylamine; trichlorophosphate; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm060142p