CarbaMic acid, N-[cis-4-[[(4-Methylphenyl)sulfonyl]oxy]cyclohexyl]-, 1,1-diMethylethyl ester

Base Information

• Chemical Name: CarbaMic acid, N-[cis-4-[[(4-Methylphenyl)sulfonyl]oxy]cyclohexyl]-, 1,1-diMethylethyl ester
• CAS No.: 1024015-36-8
• Molecular Formula: C₁₈H₂₇NO₅S
• Molecular Weight: 369.482
• Mol file: 1024015-36-8.mol

Synonyms:(1s,4s)-4-((tert-butoxycarbonyl)amino)cyclohexyl 4-methylbenzenesulfonate

Chemical Property of CarbaMic acid, N-[cis-4-[[(4-Methylphenyl)sulfonyl]oxy]cyclohexyl]-, 1,1-diMethylethyl ester

Chemical Property:

• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

cis-4-((tert-Butoxycarbonyl)amino)cyclohexyl4-methylbenzenesulfonate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of CarbaMic acid, N-[cis-4-[[(4-Methylphenyl)sulfonyl]oxy]cyclohexyl]-, 1,1-diMethylethyl ester

There total 2 articles about CarbaMic acid, N-[cis-4-[[(4-Methylphenyl)sulfonyl]oxy]cyclohexyl]-, 1,1-diMethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

cis-(4-hydroxycyclohexyl)carbamic acid tert-butyl ester (167081-25-6) + p-toluenesulfonyl chloride (98-59-9) → (1s,4s)-4-((tert-butoxycarbonyl)amino)cyclohexyl 4-methylbenzenesulfonate (1024015-36-8,1017241-31-4)

Guidance literature:

With pyridine; dmap; at 20 ℃;

DOI:10.1016/j.bmcl.2018.07.042

Reference yield:

→ (1s,4s)-4-((tert-butoxycarbonyl)amino)cyclohexyl 4-methylbenzenesulfonate (1024015-36-8,1017241-31-4)

Guidance literature:

Reference yield:

(1s,4s)-4-((tert-butoxycarbonyl)amino)cyclohexyl 4-methylbenzenesulfonate (1024015-36-8,1017241-31-4) + 2-(2,6-dichlorophenyl)-9-(1H-pyrazol-4-yl)imidazo[2,1-f][1,6]naphthyridine → (1r,4r)-4-(4-(2-(2,6-dichlorophenyl)imidazo[2,1-f][1,6]naphthyridin-9-yl)-1H-pyrazol-1-yl)cyclohexan-1-amine

Guidance literature:

With caesium carbonate; In acetonitrile; at 80 ℃; for 2h; Sealed tube;

upstream raw materials:

cis-(4-hydroxycyclohexyl)carbamic acid tert-butyl ester

p-toluenesulfonyl chloride

Downstream raw materials:

C₂₄H₂₃F₃N₄O₃S

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