Technology Process of C31H48N2O3
There total 1 articles about C31H48N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 11 steps
1.1: thionyl chloride / benzene / 3 h / Reflux
2.1: benzene
3.1: potassium carbonate / methanol; water / Reflux
3.2: pH 7
4.1: pyridinium chlorochromate / dichloromethane / 20 °C
5.1: sodium hydride / toluene / 20 °C / Cooling with ice
6.1: hydroxylamine hydrochloride / ethanol; water / Reflux
7.1: sodium methylate / methanol; diethyl ether / 0 - 20 °C
8.1: sodium tetrahydroborate / methanol / 0 °C
9.1: potassium hydroxide / methanol; water / Reflux
9.2: pH 7
10.1: thionyl chloride / benzene / 3 h / Reflux
11.1: sodium azide / acetone; benzene
With
sodium tetrahydroborate; thionyl chloride; sodium azide; hydroxylamine hydrochloride; sodium methylate; sodium hydride; potassium carbonate; pyridinium chlorochromate; potassium hydroxide;
In
methanol; diethyl ether; ethanol; dichloromethane; water; acetone; toluene; benzene;
DOI:10.1016/j.ejmech.2011.01.061