1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propane

Base Information

Chemical Name:1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propane
CAS No.:1240790-32-2
Molecular Formula:C₁₆H₂₅BO₃
Molecular Weight:276.184
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propane

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Technology Process of 1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propane

There total 3 articles about 1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 140-67-0
Estragole

: 73183-34-3
bis(pinacol)diborane

: 1240790-32-2
1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propane

Guidance literature:: With palladium diacetate; acetic acid; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine; In acetonitrile; at 90 ℃; for 24h; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1039/c7cc09432a

Reference yield: 79.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 1227056-26-9
2,2'-(propane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 1240790-32-2
1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propane

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; potassium hydroxide; In 1,4-dioxane; water; at 25 ℃; chemoselective reaction;
DOI:10.1021/ja105176v

Reference yield:

: 140-67-0
Estragole

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1240790-32-2
1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propane

: 2-(3-(4-methoxyphenyl)propyl)-4,4,5-trimethyl-1,3,2-dioxaborolane

Guidance literature:: Estragole; With (PPh₃)3CoH(N₂); In tetrahydrofuran; at 23 ℃; for 1h;

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; With (PPh₃)3CoH(N₂); In tetrahydrofuran; at 23 ℃; for 1h; Overall yield = 81 %; Overall yield = 123 mg;
DOI:10.1021/acs.orglett.5b01135