(2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide

Base Information

Chemical Name:(2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide
CAS No.:405095-67-2
Molecular Formula:C₂₃H₂₉ClN₂O₄S
Molecular Weight:465.013
Hs Code.:

Synonyms:(2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide

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Chemical Property of (2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide

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Technology Process of (2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide

There total 1 articles about (2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 256650-55-2
(2E,4R,5R)-6-Benzyloxy-N-methyl-4,5-[(2,4,6-trimethylphenylsulfonyl)epimino]hex-2-enamide

: 405095-67-2
(2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 0.5h;
DOI:10.1039/b103833h

Reference yield: 93.0%

: 5029-66-3
methyl 3-iodopropanoate

: 405095-67-2
(2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide

: Mts-L-Ser(OBn)-ψ[(E)-CH=CH]-D-Glu(OMe)-NHMe

Guidance literature:: methyl 3-iodopropanoate; With zinc; In tetrahydrofuran; at 20 ℃; for 1h;

With lithium chloride; In tetrahydrofuran; at -78 - 0 ℃;

(2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1039/b103833h

Reference yield: 78.0%

: 93415-08-8
Benzyl 3-iodopropanoate

: 405095-67-2
(2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide

: Mts-L-Ser(OBn)-ψ[(E)-CH=CH]-D-Glu(OBn)-NHMe

Guidance literature:: Benzyl 3-iodopropanoate; With zinc; In tetrahydrofuran; at 20 ℃; for 1h;

With lithium chloride; In tetrahydrofuran; at -78 - 0 ℃;

(2E,4S,5S)-6-benzyloxy-4-chloro-N-methyl-5-(2,4,6-trimethylphenylsulfonylamino)hex-2-enamide; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1039/b103833h