Technology Process of 2,2,4,4,8,8,10,10,12,12-decamethyl-2,4,6,8,10,12-hexasila-1,3,5,7,9,11,13-heptaoxaspiro<5.7>tridecane
There total 1 articles about 2,2,4,4,8,8,10,10,12,12-decamethyl-2,4,6,8,10,12-hexasila-1,3,5,7,9,11,13-heptaoxaspiro<5.7>tridecane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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17865-81-5
2,2,4,4,8,8,10,10-octamethyl-2,4,6,8,10-pentasila-1,3,5,7,9,11-hexaoxaspiro<5.5>undecane
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17995-45-8
2,2,4,4,8,8,10,10,12,12-decamethyl-2,4,6,8,10,12-hexasila-1,3,5,7,9,11,13-heptaoxaspiro<5.7>tridecane
- Guidance literature:
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With
water;
In
water; toluene; butan-1-ol;
(CH3)2SiCl2 and SiCl4 (5:1 mol) in butanol-H2O-toluene; heating of the oily product at 350-600°C in a slow stream of N2;; fractional distn.; crystn. on cooling; recrystn. from toluene;;
DOI:10.1021/ja01207a003