C₂₆H₄₁NO₃Si

Base Information

Chemical Name:C₂₆H₄₁NO₃Si
CAS No.:1351993-12-8
Molecular Formula:C₂₆H₄₁NO₃Si
Molecular Weight:443.702
Hs Code.:

C<sub>26</sub>H<sub>41</sub>NO<sub>3</sub>Si

Synonyms:C₂₆H₄₁NO₃Si

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Chemical Property of C₂₆H₄₁NO₃Si

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Technology Process of C₂₆H₄₁NO₃Si

There total 7 articles about C₂₆H₄₁NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₃₉NO₃Si

: 1351993-12-8
C₂₆H₄₁NO₃Si

Guidance literature:: With sodium tetrahydroborate; In methanol; dimethyl sulfoxide; at 0 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.09.017

Reference yield:

: C₂₁H₂₅NO₃

: 1351993-12-8
C₂₆H₄₁NO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 8 h

2: 1H-imidazole / dichloromethane / 0 - 20 °C / Inert atmosphere

3: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / 0 - 20 °C / Inert atmosphere

4: L-proline / dimethyl sulfoxide / 1 h / 25 °C / Inert atmosphere

5: sodium tetrahydroborate / methanol; dimethyl sulfoxide / 0.17 h / 0 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride; L-proline; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene;
DOI:10.1016/j.tetasy.2011.09.017

Reference yield:

: C₁₈H₂₁NO₂

: 1351993-12-8
C₂₆H₄₁NO₃Si

Guidance literature:: Multi-step reaction with 6 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / dimethyl sulfoxide / 1 h / 0 - 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 8 h

3: 1H-imidazole / dichloromethane / 0 - 20 °C / Inert atmosphere

4: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / 0 - 20 °C / Inert atmosphere

5: L-proline / dimethyl sulfoxide / 1 h / 25 °C / Inert atmosphere

6: sodium tetrahydroborate / methanol; dimethyl sulfoxide / 0.17 h / 0 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; L-proline; lithium chloride; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene; 1: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.tetasy.2011.09.017