3-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-α-D-mannopyranosyl chloride

Base Information

Chemical Name:3-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-α-D-mannopyranosyl chloride
CAS No.:219313-16-3
Molecular Formula:C₂₂H₂₄ClN₃O₅
Molecular Weight:445.903
Hs Code.:

Synonyms:3-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-α-D-mannopyranosyl chloride

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Chemical Property of 3-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-α-D-mannopyranosyl chloride

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Technology Process of 3-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-α-D-mannopyranosyl chloride

There total 1 articles about 3-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-α-D-mannopyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1,3-di-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-D-mannopyranose

: 219313-16-3
3-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-α-D-mannopyranosyl chloride

Guidance literature:: With hydrogenchloride; In diethyl ether; for 2h; Ambient temperature;
DOI:10.1016/S0008-6215(98)00219-5

Reference yield: 82.5%

: 219313-16-3
3-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-α-D-mannopyranosyl chloride

: 219313-17-4
1,3-anhydro-2-azido-4,6-di-O-benzyl-2-deoxy-β-D-mannopyranose

Guidance literature:: With potassium tert-butylate; In various solvent(s); for 6h; Ambient temperature;
DOI:10.1016/S0008-6215(98)00219-5

Reference yield:

: 219313-16-3
3-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-α-D-mannopyranosyl chloride

: 219313-13-0
methyl 3-O-acetyl-2-azido-4,6-di-O-benzyl-2-deoxy-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 82.5 percent / K-tert-butoxide / various solvent(s) / 6 h / Ambient temperature

2: 92 percent / ZnCl₂ / methanol / 4 h / Ambient temperature

3: pyridine / 4 h / Ambient temperature

With pyridine; potassium tert-butylate; zinc(II) chloride; In methanol;
DOI:10.1016/S0008-6215(98)00219-5