Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala

Base Information

Chemical Name:Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala
CAS No.:676591-50-7
Molecular Formula:C₃₇H₅₁N₅O₁₁S
Molecular Weight:773.905
Hs Code.:

Synonyms:Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala

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Chemical Property of Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala

Chemical Property:

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Technology Process of Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala

There total 20 articles about Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: N-Cbz-D-Ser[N-Boc-L-Ala-N-Me-L-Cys(Bam)-N-Me-L-Val]-OAll

: 676591-50-7
Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine; N-methylaniline; In tetrahydrofuran; at 20 ℃; for 17h; Inert atmosphere; Darkness;
DOI:10.1039/c5ob02505b

Reference yield:

: 45170-31-8
Boc-N-Me-Val-OH

: 676591-50-7
Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / DCC; N-hydroxybenzotriazole; pyridine

2: CF₃CO₂H / CH₂Cl₂

3: 74 percent / DCC; N-hydroxybenzotriazole

4: CF₃CO₂H / CH₂Cl₂

5: Zn; aq. acetic acid

With pyridine; benzotriazol-1-ol; acetic acid; dicyclohexyl-carbodiimide; trifluoroacetic acid; zinc; In dichloromethane;
DOI:10.1016/j.bmcl.2003.09.086

Reference yield:

: C₃₂H₄₂N₄O₈S

: 676591-50-7
Cbz-D-Ser-L-MeVal-L-MeCys(Bam)-Boc-L-Ala

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / N,N-dimethyl-formamide / 21 h / 20 °C / Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine; N-methylaniline / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere; Darkness

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine; N-methylaniline; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c5ob02505b