{2-(3)H}toluene

Base Information

• Chemical Name: {2-(3)H}toluene
• CAS No.: 54615-78-0
• Molecular Formula: C₇H₈
• Molecular Weight: 94.1326
• Mol file: 54615-78-0.mol

Synonyms:{2-(3)H}toluene

Chemical Property of {2-(3)H}toluene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {2-(3)H}toluene

There total 2 articles about {2-(3)H}toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

toluene (108-88-3,15644-74-3,16713-13-6) → [3-3H]toluene (6726-72-3) + {2-(3)H}toluene (54615-78-0) + α-Tritiotoluol (6683-73-4) + 4-tritio-toluene (40661-90-3)

Guidance literature:

With tritium; Pt-Y-zeolite; In gas; at 100 ℃; for 72h; Product distribution; other hydrocarbons, var. catalysts, temp. and time;

Reference yield:

→ {2-(3)H}toluene (54615-78-0)

Guidance literature:

Haloaromat, 1.) Mg, 2.) T2O;

Reference yield:

{2-(3)H}toluene (54615-78-0) + sodium chloride (7647-14-5) + mercury(II) oxide (12653-71-3) → p-chloromercuri{2-(3)H}toluene (142414-88-8)

Guidance literature:

In perchloric acid; acetic acid; stirring (3)H-labelled toluene (from o-bromotoluene and (3)H2) and HgO in glacial acetic acid and 30% HClO4 for 6h, removal of acetic acid and excess of (3)H-labelled toluene, addn. of 1M NaCl-soln. to the residue, pptn.;; cooling to -3°C for 3h, centrifugation, washing with H2O, drying in a rotary evaporator;;

upstream raw materials:

toluene

Downstream raw materials:

p-chloromercuri{2-⁽³⁾H}toluene