5-methoxy-1-triethylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Base Information

Chemical Name:5-methoxy-1-triethylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene
CAS No.:1160553-84-3
Molecular Formula:C₁₉H₃₃BO₃Si
Molecular Weight:348.366
Hs Code.:

Synonyms:5-methoxy-1-triethylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Suppliers and Price of 5-methoxy-1-triethylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-methoxy-1-triethylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-methoxy-1-triethylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

There total 4 articles about 5-methoxy-1-triethylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1160553-72-9
CH₃OC₆H₃B(N₃HC₉H₆)Si(C₂H₅)3

: 1160553-84-3
5-methoxy-1-triethylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Guidance literature:: With CH₃C₆H₄SO₃H; In toluene; pinacol, toluene, TsOH;

Reference yield: 75.0%

: 617-86-7
triethylsilane

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 5720-07-0
4-methoxyphenylboronic acid

: 1160553-84-3
5-methoxy-1-triethylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Guidance literature:: 4-methoxyphenylboronic acid; With 5-(2-aminophenyl)-1H-pyrazole; In toluene; for 1h; Inert atmosphere; Reflux; Dean-Stark;

triethylsilane; With norborn-2-ene; carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); In toluene; at 20 - 135 ℃; for 12h; Inert atmosphere;

2,3-dimethyl-2,3-butane diol; With toluene-4-sulfonic acid; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1021/jo402174v

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 1160553-84-3
5-methoxy-1-triethylsilyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 5-(2-aminophenyl)-1H-pyrazole / toluene / 1 h / Reflux; Dean-Stark

1.2: 12 h / 135 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / tetrahydrofuran / 20 °C

With toluene-4-sulfonic acid; 5-(2-aminophenyl)-1H-pyrazole; In tetrahydrofuran; toluene;