(+/-)-N²-(monomethoxytrityl)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine

Base Information

Chemical Name:(+/-)-N²-(monomethoxytrityl)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine
CAS No.:188949-77-1
Molecular Formula:C₃₄H₃₃N₅O₄
Molecular Weight:575.667
Hs Code.:

(+/-)-N<sup>2</sup>-(monomethoxytrityl)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine

Synonyms:(+/-)-N²-(monomethoxytrityl)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine

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Chemical Property of (+/-)-N²-(monomethoxytrityl)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine

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Technology Process of (+/-)-N²-(monomethoxytrityl)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine

There total 4 articles about (+/-)-N²-(monomethoxytrityl)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 188949-72-6
(+/-)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine

: 14470-28-1
mono-4-methoxytrityl chloride

: 188949-77-1
(+/-)-N²-(monomethoxytrityl)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine

Guidance literature:: With pyridine; at 60 ℃;
DOI:10.1021/jo962204x

Reference yield:

: 3725-40-4
ethyl 1,3-cyclohexadiene-1-carboxylate

: 188949-77-1
(+/-)-N²-(monomethoxytrityl)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / DBU / dimethylformamide / 48 h / 75 °C

2: 85 percent / CF₃CO₂H, H₂O / 48 h / Ambient temperature

3: 80 percent / pyridine / 60 °C

With pyridine; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jo962204x

Reference yield:

: 10310-21-1
2-Amino-6-chloropurin

: 188949-77-1
(+/-)-N²-(monomethoxytrityl)-9-[4-(ethoxycarbonyl)-3-cyclohexenyl]guanine

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / DBU / dimethylformamide / 48 h / 75 °C

2: 85 percent / CF₃CO₂H, H₂O / 48 h / Ambient temperature

3: 80 percent / pyridine / 60 °C

With pyridine; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jo962204x