cis-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid

Base Information

• Chemical Name: cis-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid
• CAS No.: 135524-54-8
• Molecular Formula: C₁₀H₉ClF₆O
• Molecular Weight: 294.624

Synonyms:cis-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid

Chemical Property of cis-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid

Chemical Property:

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Technology Process of cis-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid

There total 2 articles about cis-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl (dimethylsulfuranylidene)acetate (7380-81-6) + 4-Chlor-1,1,1-trifluor-5-methyl-2-(trifluormethyl)-2-hexen (99903-41-0) → dimethylsulfide (75-18-3) + cis-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid (135524-54-8) + trans-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid (121618-27-7,135524-54-8)

Guidance literature:

Yield given. Title compound not separated from byproducts;

Reference yield:

ethyl (dimethylsulfuranylidene)acetate (7380-81-6) + 4-Chlor-1,1,1-trifluor-5-methyl-2-(trifluormethyl)-2-hexen (99903-41-0) → dimethylsulfide (75-18-3) + cis-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid (135524-54-8) + trans-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid (121618-27-7,135524-54-8)

Guidance literature:

Yield given. Title compound not separated from byproducts;

Reference yield: 87.0%

2-hydroxy-2-(3-phenoxyphenyl)acetonitrile (39515-47-4) + trans-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeurechlorid (121618-27-7,135524-54-8) → trans-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeure-(α-cyan-3-phenoxybenzyl)ester (99903-55-6,121701-44-8,121701-47-1,135635-76-6,135635-77-7)

Guidance literature:

With pyridine; In toluene; for 72h; Ambient temperature;

upstream raw materials:

ethyl (dimethylsulfuranylidene)acetate

4-Chlor-1,1,1-trifluor-5-methyl-2-(trifluormethyl)-2-hexen

Downstream raw materials:

cis-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeure-(α-cyan-3-phenoxybenzyl)ester

trans-3-(2-Methyl-1-propenyl)-2,2-bis(trifluormethyl)cyclopropancarbonsaeure-(α-cyan-3-phenoxybenzyl)ester

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