propyl 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazol-5-yl))biphenyl-4-yl]methyl]imidazole-5-carboxylate

Base Information

• Chemical Name: propyl 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazol-5-yl))biphenyl-4-yl]methyl]imidazole-5-carboxylate
• CAS No.: 154749-90-3
• Molecular Formula: C₄₅H₄₄N₆O₂
• Molecular Weight: 700.883

Synonyms:propyl 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazol-5-yl))biphenyl-4-yl]methyl]imidazole-5-carboxylate

Chemical Property of propyl 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazol-5-yl))biphenyl-4-yl]methyl]imidazole-5-carboxylate

Chemical Property:

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Technology Process of propyl 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazol-5-yl))biphenyl-4-yl]methyl]imidazole-5-carboxylate

There total 2 articles about propyl 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazol-5-yl))biphenyl-4-yl]methyl]imidazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-iodo-propane (107-08-4) + 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazole-5-yl))biphenyl-4-yl]methyl]-imidazole-5-carboxylate (154749-89-0) → propyl 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazol-5-yl))biphenyl-4-yl]methyl]imidazole-5-carboxylate (154749-90-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 24h;

DOI:10.1023/A:1016228129729

Reference yield:

4-ethyl-2-n-propyl-1-((2'-(1H-tetrazol-5-yl)biphenyl-4-yl)-methyl)imidazole-5-carboxylic acid (139964-19-5) → propyl 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazol-5-yl))biphenyl-4-yl]methyl]imidazole-5-carboxylate (154749-90-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 6.46 g / Et₃N / CH₂Cl₂

2: 0.96 g / K₂CO₃ / dimethylformamide / 24 h

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 1: Alkylation / 2: Esterification;

DOI:10.1023/A:1016228129729

Reference yield:

propyl 4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazol-5-yl))biphenyl-4-yl]methyl]imidazole-5-carboxylate (154749-90-3) → propyl 4-ethyl-2-propyl-1-[[2'-(tetrazol-5-yl)biphenyl-4-yl]methyl]imidazole-5-carboxylate

Guidance literature:

With hydrogenchloride; silica gel; In methanol; for 72h;

DOI:10.1023/A:1016228129729

upstream raw materials:

1-iodo-propane

4-ethyl-2-propyl-1-[[2'-(N-triphenylmethyl(tetrazole-5-yl))biphenyl-4-yl]methyl]-imidazole-5-carboxylate

4-ethyl-2-n-propyl-1-((2'-(1H-tetrazol-5-yl)biphenyl-4-yl)-methyl)imidazole-5-carboxylic acid

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