BETA-OXO-BENZENEHEPTANOIC ACID 1,1-DIMETHYLETHYL ESTER

Base Information

Chemical Name:BETA-OXO-BENZENEHEPTANOIC ACID 1,1-DIMETHYLETHYL ESTER
CAS No.:189030-32-8
Molecular Formula:C₁₇H₂₄O₃
Molecular Weight:276.376
Hs Code.:

Synonyms:tert-butyl 3-oxo-7-phenylheptanoate

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Chemical Property of BETA-OXO-BENZENEHEPTANOIC ACID 1,1-DIMETHYLETHYL ESTER

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Technology Process of BETA-OXO-BENZENEHEPTANOIC ACID 1,1-DIMETHYLETHYL ESTER

There total 3 articles about BETA-OXO-BENZENEHEPTANOIC ACID 1,1-DIMETHYLETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 150942-98-6
t-butyl lithioacetate

: 55628-85-8
1-Imidazol-1-yl-5-phenyl-pentan-1-one

: 189030-32-8
tert-butyl 3-oxo-7-phenylheptanoate

Guidance literature:: at -78 ℃; for 1h;
DOI:10.1039/a901921i

Reference yield:

: 540-88-5
acetic acid tert-butyl ester

: C₁₅H₁₆N₂O₃

: 189030-32-8
tert-butyl 3-oxo-7-phenylheptanoate

Guidance literature:: acetic acid tert-butyl ester; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h;

C₁₅H₁₆N₂O₃; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1039/b401435a

Reference yield:

: 2270-20-4
5-Phenylpentanoic acid

: 150942-98-6
t-butyl lithioacetate

: 189030-32-8
tert-butyl 3-oxo-7-phenylheptanoate

Guidance literature:: With 1,1'-carbonyldiimidazole; Yield given. Multistep reaction; 1.) THF, 0 deg C, 0.5 h; room temperature, overnight, 2.) THF, hexane, -78 deg C, 0.5 h;
DOI:10.1016/S0968-0896(98)00009-1