(E)-mesitaldehyde oxime

Base Information

Chemical Name:(E)-mesitaldehyde oxime
CAS No.:54130-63-1
Molecular Formula:C₁₀H₁₃NO
Molecular Weight:163.219
Hs Code.:

Synonyms:(E)-mesitaldehyde oxime

Suppliers and Price of (E)-mesitaldehyde oxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of (E)-mesitaldehyde oxime

Chemical Property:

Purity/Quality:: 98%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (E)-mesitaldehyde oxime

There total 6 articles about (E)-mesitaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 909786-08-9
(R)-3-Phenyl-3-{[1-(2,4,6-trimethyl-phenyl)-meth-(E)-ylidene]-amino}-propionic acid tert-butyl ester

: 54130-62-0
(Z)-2,4,6-trimethybenzaldehyde oxime

: 54130-63-1
(E)-mesitaldehyde oxime

: 161671-34-7
tert-butyl (R)-3-amino-3-phenylpropionate

Guidance literature:: With hydroxylamine hydrochloride; In tetrahydrofuran; water; at 20 ℃; for 0.25h;
DOI:10.1016/j.tet.2006.06.040

Reference yield:

: 909849-55-4
N-(mesitylmethyl)-N-(trimethylsilyl)amine

: 54130-63-1
(E)-mesitaldehyde oxime

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / n-BuLi; (-)-(R,R)-(CH₃OCH(Ph))2 / toluene; hexane / 2.5 h / -78 °C

2: 99 percent / NCS / CH₂Cl₂ / 14 h / -20 °C

3: HN=C(NMe₂)2 / benzene / 17 h / 20 °C

4: NH₂OH*HCl / tetrahydrofuran; H₂O / 0.25 h / 20 °C

With N-chloro-succinimide; n-butyllithium; (1R,2R)-1,2-diphenyl-1,2-dimethoxyethane; hydroxylamine hydrochloride; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; hexane; dichloromethane; water; toluene; benzene;
DOI:10.1016/j.tet.2006.06.040

Reference yield:

: 909786-02-3
(+)-tert-butyl (R)-3-((mesitylmethyl)amino)-3-phenylpropanoate

: 54130-63-1
(E)-mesitaldehyde oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NCS / CH₂Cl₂ / 14 h / -20 °C

2: HN=C(NMe₂)2 / benzene / 17 h / 20 °C

3: NH₂OH*HCl / tetrahydrofuran; H₂O / 0.25 h / 20 °C

With N-chloro-succinimide; hydroxylamine hydrochloride; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; dichloromethane; water; benzene;
DOI:10.1016/j.tet.2006.06.040