3,4,5-Tris-dodecyloxy-benzoic acid 4-(4-carboxy-phenoxycarbonyl)-phenyl ester

Base Information

• Chemical Name: 3,4,5-Tris-dodecyloxy-benzoic acid 4-(4-carboxy-phenoxycarbonyl)-phenyl ester
• CAS No.: 187584-97-0
• Molecular Formula: C₅₇H₈₆O₉
• Molecular Weight: 915.304

Synonyms:3,4,5-Tris-dodecyloxy-benzoic acid 4-(4-carboxy-phenoxycarbonyl)-phenyl ester

Chemical Property of 3,4,5-Tris-dodecyloxy-benzoic acid 4-(4-carboxy-phenoxycarbonyl)-phenyl ester

Chemical Property:

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Technology Process of 3,4,5-Tris-dodecyloxy-benzoic acid 4-(4-carboxy-phenoxycarbonyl)-phenyl ester

There total 5 articles about 3,4,5-Tris-dodecyloxy-benzoic acid 4-(4-carboxy-phenoxycarbonyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3,4,5-Tris-dodecyloxy-benzoic acid 4-(4-benzyloxycarbonyl-phenoxycarbonyl)-phenyl ester → 3,4,5-Tris-dodecyloxy-benzoic acid 4-(4-carboxy-phenoxycarbonyl)-phenyl ester (187584-97-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; Ambient temperature;

DOI:10.1002/anie.199701501

Reference yield:

Benzyl 4-hydroxybenzoate (94-18-8) → 3,4,5-Tris-dodecyloxy-benzoic acid 4-(4-carboxy-phenoxycarbonyl)-phenyl ester (187584-97-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 92 percent / DMAP, DCC, molecular sieves / CH₂Cl₂; tetrahydrofuran / Ambient temperature

2: 75 percent / H₂ / 10percent Pd/C / tetrahydrofuran / Ambient temperature

3: 97 percent / DMAP, DCC, molecular sieves / CH₂Cl₂; tetrahydrofuran / Ambient temperature

4: 86 percent / H₂ / 10percent Pd/C / tetrahydrofuran / Ambient temperature

With dmap; molecular sieve; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;

DOI:10.1002/anie.199701501

Reference yield:

3,4,5-tridodecyloxy benzoic acid (117241-31-3) → 3,4,5-Tris-dodecyloxy-benzoic acid 4-(4-carboxy-phenoxycarbonyl)-phenyl ester (187584-97-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 92 percent / DMAP, DCC, molecular sieves / CH₂Cl₂; tetrahydrofuran / Ambient temperature

2: 75 percent / H₂ / 10percent Pd/C / tetrahydrofuran / Ambient temperature

3: 97 percent / DMAP, DCC, molecular sieves / CH₂Cl₂; tetrahydrofuran / Ambient temperature

4: 86 percent / H₂ / 10percent Pd/C / tetrahydrofuran / Ambient temperature

With dmap; molecular sieve; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;

DOI:10.1002/anie.199701501

upstream raw materials:

Benzyl 4-hydroxybenzoate

3,4,5-tridodecyloxy benzoic acid

4-[3',4',5'-tris(dodecyloxy)benzoyloxy]benzoic acid

Downstream raw materials:

C₁₇₇H₂₅₈O₂₇

1,3,5-tris(3,4,5-tridodecyloxybenzoyloxy-4'-benzoyloxy-4''-benzoyloxy)-2,4,6-triiodobenzene

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