2-(4-butoxy-benzenesulfonylamino)-5-[3-(3-chloro-2-fluoro-benzene-sulfonylaminocarbonyl)-phenoxy]-benzoic acid

Base Information

Chemical Name:2-(4-butoxy-benzenesulfonylamino)-5-[3-(3-chloro-2-fluoro-benzene-sulfonylaminocarbonyl)-phenoxy]-benzoic acid
CAS No.:1192315-87-9
Molecular Formula:C₃₀H₂₆ClFN₂O₉S₂
Molecular Weight:677.128
Hs Code.:

Synonyms:2-(4-butoxy-benzenesulfonylamino)-5-[3-(3-chloro-2-fluoro-benzene-sulfonylaminocarbonyl)-phenoxy]-benzoic acid

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Chemical Property of 2-(4-butoxy-benzenesulfonylamino)-5-[3-(3-chloro-2-fluoro-benzene-sulfonylaminocarbonyl)-phenoxy]-benzoic acid

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Technology Process of 2-(4-butoxy-benzenesulfonylamino)-5-[3-(3-chloro-2-fluoro-benzene-sulfonylaminocarbonyl)-phenoxy]-benzoic acid

There total 2 articles about 2-(4-butoxy-benzenesulfonylamino)-5-[3-(3-chloro-2-fluoro-benzene-sulfonylaminocarbonyl)-phenoxy]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1192317-93-3
C₃₄H₃₄ClFN₂O₉S₂

: 1192315-87-9
2-(4-butoxy-benzenesulfonylamino)-5-[3-(3-chloro-2-fluoro-benzene-sulfonylaminocarbonyl)-phenoxy]-benzoic acid

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 20h;

Reference yield:

: 351003-58-2
3-chloro-2-fluorobenzenesulfonamide

: C₂₈H₃₁NO₈S

: 1192315-87-9
2-(4-butoxy-benzenesulfonylamino)-5-[3-(3-chloro-2-fluoro-benzene-sulfonylaminocarbonyl)-phenoxy]-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 h / 20 °C

2: triethylsilane; trifluoroacetic acid / dichloromethane / 20 h / 20 °C

With triethylsilane; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;