C₃₃H₄₀N₄O₆Si

Base Information

Chemical Name:C₃₃H₄₀N₄O₆Si
CAS No.:1295471-19-0
Molecular Formula:C₃₃H₄₀N₄O₆Si
Molecular Weight:616.789
Hs Code.:

C<sub>33</sub>H<sub>40</sub>N<sub>4</sub>O<sub>6</sub>Si

Synonyms:C₃₃H₄₀N₄O₆Si

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Chemical Property of C₃₃H₄₀N₄O₆Si

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Technology Process of C₃₃H₄₀N₄O₆Si

There total 14 articles about C₃₃H₄₀N₄O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1295471-59-8
C₁₇H₂₂N₄O₆

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1295471-19-0
C₃₃H₄₀N₄O₆Si

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 4h;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-56-5
C₁₇H₂₀N₄O₅

: 1295471-19-0
C₃₃H₄₀N₄O₆Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: zinc trifluoromethanesulfonate; acetic acid / 48 h / 80 °C

1.2: 1 h / 0 - 20 °C

2.1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C

With dmap; zinc trifluoromethanesulfonate; acetic acid; triethylamine; In dichloromethane;
DOI:10.1002/anie.201008079

Reference yield:

: L-threonine

: 1295471-19-0
C₃₃H₄₀N₄O₆Si

Guidance literature:: Multi-step reaction with 20 steps

1: thionyl chloride / acetonitrile / 0 - 20 °C

2: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

3: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

4: diisobutylaluminium hydride / dichloromethane / -78 °C

5: methylmagnesium bromide / diethyl ether / 0 °C

6: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C

7: ozone / dichloromethane / -78 °C

8: N-ethyl-N,N-diisopropylamine; titanium tetrachloride; chloro-trimethyl-silane / dichloromethane / 0 °C

9: trifluoroacetyl chloride; pyridine / dichloromethane / 20 °C

10: dihydrogen peroxide; sodium hydroxide / methanol; dichloromethane / 0 °C

11: cerium(III) chloride heptahydrate; sodium tetrahydroborate / methanol; dichloromethane / 0 °C

12: pyridine / -78 - 0 °C

13: tetrabutylammoniun azide / toluene / 20 °C

14: trifluoroacetic acid / acetonitrile; water / 0 - 20 °C

15: Dess-Martin periodane / dichloromethane / 0 - 20 °C

16: tetrahydrofuran / -78 °C

17: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

18: zinc trifluoromethanesulfonate; acetic acid / 80 °C

19: potassium carbonate / methanol / 20 °C

20: triethylamine; dmap / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; sodium tetrahydroborate; chloro-trimethyl-silane; thionyl chloride; oxalyl dichloride; cerium(III) chloride heptahydrate; methylmagnesium bromide; tetrabutyl ammonium fluoride; dihydrogen peroxide; tetrabutylammoniun azide; titanium tetrachloride; zinc trifluoromethanesulfonate; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; ozone; acetic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; trifluoroacetyl chloride; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/jo301638z