1-(5'-benzyloxy-4'-methoxy-2'-nitrobenzyl)-3,4-dihydro-5,6-dimethoxydihydroisoquinoline

Base Information

Chemical Name:1-(5'-benzyloxy-4'-methoxy-2'-nitrobenzyl)-3,4-dihydro-5,6-dimethoxydihydroisoquinoline
CAS No.:78792-66-2
Molecular Formula:C₂₆H₂₆N₂O₆
Molecular Weight:462.502
Hs Code.:

Synonyms:1-(5'-benzyloxy-4'-methoxy-2'-nitrobenzyl)-3,4-dihydro-5,6-dimethoxydihydroisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(5'-benzyloxy-4'-methoxy-2'-nitrobenzyl)-3,4-dihydro-5,6-dimethoxydihydroisoquinoline

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Technology Process of 1-(5'-benzyloxy-4'-methoxy-2'-nitrobenzyl)-3,4-dihydro-5,6-dimethoxydihydroisoquinoline

There total 5 articles about 1-(5'-benzyloxy-4'-methoxy-2'-nitrobenzyl)-3,4-dihydro-5,6-dimethoxydihydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 78792-75-3
N-<3,4-Dimethoxyphenethyl>-5-benzyloxy-4-methoxy-2-nitrophenylacetamide

: 78792-66-2
1-(5'-benzyloxy-4'-methoxy-2'-nitrobenzyl)-3,4-dihydro-5,6-dimethoxydihydroisoquinoline

Guidance literature:: With phosphorus pentachloride; In dichloromethane; at 0 ℃; for 1h; stirred at r.t. overnight;
DOI:10.1002/jhet.5570180226

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 78792-66-2
1-(5'-benzyloxy-4'-methoxy-2'-nitrobenzyl)-3,4-dihydro-5,6-dimethoxydihydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / standing overnight

2: 87 percent / phosphorus pentachloride / CH₂Cl₂ / 1 h / 0 °C / stirred at r.t. overnight

With phosphorus pentachloride; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1002/jhet.5570180226

Reference yield:

: 78792-73-1
5-benzyloxy-4-methoxy-2-nitrophenylacetic acid

: 78792-66-2
1-(5'-benzyloxy-4'-methoxy-2'-nitrobenzyl)-3,4-dihydro-5,6-dimethoxydihydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / standing overnight

2: 87 percent / phosphorus pentachloride / CH₂Cl₂ / 1 h / 0 °C / stirred at r.t. overnight

With phosphorus pentachloride; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1002/jhet.5570180226