1-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-phenylsemicarbazide

Base Information

Chemical Name:1-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-phenylsemicarbazide
CAS No.:139951-47-6
Molecular Formula:C₂₁H₂₈N₄O₉
Molecular Weight:480.475
Hs Code.:

Synonyms:1-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-phenylsemicarbazide

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Chemical Property of 1-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-phenylsemicarbazide

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Technology Process of 1-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-phenylsemicarbazide

There total 4 articles about 1-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-phenylsemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 10294-12-9,10353-11-4,70749-28-9,76612-22-1,116559-73-0,147129-68-8,34051-43-9
2-deoxy-2-acetamido-3,4,6-tri-O-acetyl-D-glucopyranose

: 537-47-3
4-phenyl-semicarbazide

: 139951-48-7
2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucose 4-phenylsemicarbazone

: 139951-47-6
1-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-phenylsemicarbazide

Guidance literature:: With oxalic acid; In 1,2-dichloro-ethane; for 6h; Heating;
DOI:10.1002/hlca.19920750129

Reference yield:

: 139951-48-7
2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucose 4-phenylsemicarbazone

: 139951-47-6
1-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-phenylsemicarbazide

Guidance literature:: With acetic acid; In methanol; Yield given;
DOI:10.1002/hlca.19920750129

Reference yield:

: 10294-12-9,10353-11-4,70749-28-9,76612-22-1,116559-73-0,147129-68-8,34051-43-9
2-deoxy-2-acetamido-3,4,6-tri-O-acetyl-D-glucopyranose

: 139951-47-6
1-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-phenylsemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / oxalic acid / 1,2-dichloro-ethane / 6 h / Heating

2: AcOH / methanol

With oxalic acid; acetic acid; In methanol; 1,2-dichloro-ethane;
DOI:10.1002/hlca.19920750129