2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucono-1,5-lactone 4-phenylsemicarbazone

Base Information

Chemical Name:2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucono-1,5-lactone 4-phenylsemicarbazone
CAS No.:139951-50-1
Molecular Formula:C₂₁H₂₆N₄O₉
Molecular Weight:478.459
Hs Code.:

Synonyms:2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucono-1,5-lactone 4-phenylsemicarbazone

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Chemical Property of 2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucono-1,5-lactone 4-phenylsemicarbazone

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Technology Process of 2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucono-1,5-lactone 4-phenylsemicarbazone

There total 3 articles about 2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucono-1,5-lactone 4-phenylsemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 139951-47-6
1-(2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-4-phenylsemicarbazide

: 139951-50-1
2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucono-1,5-lactone 4-phenylsemicarbazone

Guidance literature:: With chromium trioxide-pyridine complex; In dichloromethane; at 0 ℃; for 5h;
DOI:10.1002/hlca.19920750129

Reference yield:

: 537-47-3
4-phenyl-semicarbazide

: 139951-50-1
2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucono-1,5-lactone 4-phenylsemicarbazone

Guidance literature:: Multi-step reaction with 3 steps

1: 19 percent / oxalic acid / 1,2-dichloro-ethane / 6 h / Heating

2: AcOH / methanol

3: 74 percent / CrO₃-pyridine / CH₂Cl₂ / 5 h / 0 °C

With chromium trioxide-pyridine complex; oxalic acid; acetic acid; In methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/hlca.19920750129

Reference yield:

: 139951-48-7
2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucose 4-phenylsemicarbazone

: 139951-50-1
2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-D-glucono-1,5-lactone 4-phenylsemicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH / methanol

2: 74 percent / CrO₃-pyridine / CH₂Cl₂ / 5 h / 0 °C

With chromium trioxide-pyridine complex; acetic acid; In methanol; dichloromethane;
DOI:10.1002/hlca.19920750129