2-methyl-1-cyclohexenyl phenyl sulfide

Base Information

• Chemical Name: 2-methyl-1-cyclohexenyl phenyl sulfide
• CAS No.: 67957-91-9
• Molecular Formula: C₁₃H₁₆S
• Molecular Weight: 204.336

Synonyms:2-methyl-1-cyclohexenyl phenyl sulfide

Chemical Property of 2-methyl-1-cyclohexenyl phenyl sulfide

Chemical Property:

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Technology Process of 2-methyl-1-cyclohexenyl phenyl sulfide

There total 12 articles about 2-methyl-1-cyclohexenyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

thiophenol (108-98-5) + 2-Methylcyclohexanone (583-60-8) → 2-methyl-1-cyclohexenyl phenyl sulfide (67957-91-9) + 6-methyl-1-cyclohexenyl phenyl sulfide (85894-85-5)

Guidance literature:

With montmorillonite KSF; In toluene; Heating; Montmorilionite; nach Lit_.zitat;

DOI:10.1021/jo00303a004

Reference yield: 73.0%

2-Methylcyclohexanone (583-60-8) → 2-methyl-1-cyclohexenyl phenyl sulfide (67957-91-9)

Guidance literature:

Heating;

DOI:10.1021/ja027988c

Reference yield: 70.0%

thiophenol (108-98-5) + 2-Methylcyclohexanone (583-60-8) → 2-methyl-1-cyclohexenyl phenyl sulfide (67957-91-9)

Guidance literature:

With phosphorus pentoxide; In dichloromethane; for 20h; Ambient temperature;

DOI:10.1055/s-1995-4138

upstream raw materials:

thiophenol

2-Methylcyclohexanone

2-methyl-1-(phenylsulfinyl)cyclohexane

1,1-bis(phenylthio)-2-methylcyclohexane

Downstream raw materials:

2-(2-Methyl-1-phenylsulfanyl-cyclohexyl)-1-phenyl-ethanone

(1-Allyl-2-methyl-cyclohexylsulfanyl)-benzene

1-Hexyl-2-methyl-cyclohexene

1-allyl-2-methyl-cyclohexene

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