C₂₉H₂₄O

Base Information

Chemical Name:C₂₉H₂₄O
CAS No.:1453803-75-2
Molecular Formula:C₂₉H₂₄O
Molecular Weight:388.509
Hs Code.:

Synonyms:C₂₉H₂₄O

Suppliers and Price of C₂₉H₂₄O

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₉H₂₄O

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₉H₂₄O

There total 2 articles about C₂₉H₂₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 886-66-8
1,4-diphenyl-1,3-butadiyne

: 89343-06-6
tris-iso-propylsilyl acetylene

: 87959-49-7
1-(buta-2,3-dien-2-yl)-4-methoxybenzene

: 1453803-75-2
C₂₉H₂₄O

Guidance literature:: tris-iso-propylsilyl acetylene; 1-(buta-2,3-dien-2-yl)-4-methoxybenzene; With cobalt(II) acetate tetrahydrate; C₅₄H₈₀FeO₂P₂; zinc; In dimethyl sulfoxide; at 80 ℃; for 3h; Inert atmosphere;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol; at 20 ℃; for 1.5h; Inert atmosphere;

1,4-diphenyl-1,3-butadiyne; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 24h; enantioselective reaction; Inert atmosphere; Reflux;
DOI:10.1021/jo401604n

Reference yield:

: 52178-73-1
1-(2,2-dibromo-1-methylcyclopropyl)-4-methoxybenzene

: 1453803-75-2
C₂₉H₂₄O

Guidance literature:: Multi-step reaction with 2 steps

1.1: methyllithium / diethyl ether / 1.5 h / -40 °C / Inert atmosphere

2.1: zinc; C₅₄H₈₀FeO₂P₂; cobalt(II) acetate tetrahydrate / dimethyl sulfoxide / 3 h / 80 °C / Inert atmosphere

2.2: 1.5 h / 20 °C / Inert atmosphere

2.3: 24 h / 20 °C / Inert atmosphere; Reflux

With cobalt(II) acetate tetrahydrate; C₅₄H₈₀FeO₂P₂; methyllithium; zinc; In diethyl ether; dimethyl sulfoxide;
DOI:10.1021/jo401604n