C₂₄H₃₁NO₈

Base Information

Chemical Name:C₂₄H₃₁NO₈
CAS No.:1363373-57-2
Molecular Formula:C₂₄H₃₁NO₈
Molecular Weight:461.512
Hs Code.:

C<sub>24</sub>H<sub>31</sub>NO<sub>8</sub>

Synonyms:C₂₄H₃₁NO₈

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Chemical Property of C₂₄H₃₁NO₈

Chemical Property:

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Technology Process of C₂₄H₃₁NO₈

There total 10 articles about C₂₄H₃₁NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99314-44-0
(3-methyloxetan-3-yl)methyl 4-methylbenzenesulfonate

: 1363373-57-2
C₂₄H₃₁NO₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 36 h / 70 °C / Inert atmosphere

2.1: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

2.2: 0.5 h

3.1: dichloromethane / -78 °C / Inert atmosphere

3.2: 2.08 h / -78 °C / Inert atmosphere

3.3: 0.67 h / -78 - 0 °C

4.1: dichloromethane

5.1: oxalyl dichloride; dimethyl sulfoxide

6.1: -78 °C

7.1: water; acetic acid / tetrahydrofuran

With oxalyl dichloride; boron trifluoride diethyl etherate; water; tetra-(n-butyl)ammonium iodide; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 873-75-6
4-bromobenzenemethanol

: 1363373-57-2
C₂₄H₃₁NO₈

Guidance literature:: Multi-step reaction with 6 steps

1: 1H-imidazole / N,N-dimethyl-formamide

2: magnesium / tetrahydrofuran

3: dichloromethane

4: oxalyl dichloride; dimethyl sulfoxide

5: -78 °C

6: water; acetic acid / tetrahydrofuran

With 1H-imidazole; oxalyl dichloride; water; magnesium; acetic acid; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 3143-02-0
3-hydroxymethyl-3-methyloxethane

: 1363373-57-2
C₂₄H₃₁NO₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: pyridine / 1.75 h / 0 - 20 °C / Inert atmosphere

2.1: triethylamine; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 36 h / 70 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

3.2: 0.5 h

4.1: dichloromethane / -78 °C / Inert atmosphere

4.2: 2.08 h / -78 °C / Inert atmosphere

4.3: 0.67 h / -78 - 0 °C

5.1: dichloromethane

6.1: oxalyl dichloride; dimethyl sulfoxide

7.1: -78 °C

8.1: water; acetic acid / tetrahydrofuran

With pyridine; oxalyl dichloride; boron trifluoride diethyl etherate; water; tetra-(n-butyl)ammonium iodide; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;