propylcarbamic acid 2-diphenylphosphanyl-4-hydroxymethylphenyl ester

Base Information

Chemical Name:propylcarbamic acid 2-diphenylphosphanyl-4-hydroxymethylphenyl ester
CAS No.:896740-41-3
Molecular Formula:C₂₃H₂₄NO₃P
Molecular Weight:393.422
Hs Code.:

Synonyms:propylcarbamic acid 2-diphenylphosphanyl-4-hydroxymethylphenyl ester

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Chemical Property of propylcarbamic acid 2-diphenylphosphanyl-4-hydroxymethylphenyl ester

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Technology Process of propylcarbamic acid 2-diphenylphosphanyl-4-hydroxymethylphenyl ester

There total 4 articles about propylcarbamic acid 2-diphenylphosphanyl-4-hydroxymethylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 896740-40-2
propylcarbamic acid 2-diphenylphosphanyl-4-formylphenyl ester

: 896740-41-3
propylcarbamic acid 2-diphenylphosphanyl-4-hydroxymethylphenyl ester

Guidance literature:: With sodium tetrahydroborate; In chloroform; isopropyl alcohol; at 20 ℃; for 0.5h;
DOI:10.1016/j.bmcl.2006.03.073

Reference yield:

: 60032-63-5
4-hydroxy-3-iodo-benzaldehyde

: 896740-41-3
propylcarbamic acid 2-diphenylphosphanyl-4-hydroxymethylphenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 44 percent / potassium acetate; Pd(OAc)2 / acetonitrile / 130 °C

2: 91 percent / pyridine / CH₂Cl₂ / 48 h / 20 °C

3: 85 percent / NABH₄ / CHCl₃; propan-2-ol / 0.5 h / 20 °C

With pyridine; palladium diacetate; sodium tetrahydroborate; potassium acetate; In dichloromethane; chloroform; isopropyl alcohol; acetonitrile;
DOI:10.1016/j.bmcl.2006.03.073

Reference yield:

: 896740-39-9
3-diphenylphosphanyl-4-hydroxybenzaldehyde

: 896740-41-3
propylcarbamic acid 2-diphenylphosphanyl-4-hydroxymethylphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / pyridine / CH₂Cl₂ / 48 h / 20 °C

2: 85 percent / NABH₄ / CHCl₃; propan-2-ol / 0.5 h / 20 °C

With pyridine; sodium tetrahydroborate; In dichloromethane; chloroform; isopropyl alcohol;
DOI:10.1016/j.bmcl.2006.03.073