4-nitrophenylcarbonic acid 3-diphenylphosphanyl-4-propylcarbamoyloxybenzyl ester

Base Information

Chemical Name:4-nitrophenylcarbonic acid 3-diphenylphosphanyl-4-propylcarbamoyloxybenzyl ester
CAS No.:896740-42-4
Molecular Formula:C₃₀H₂₇N₂O₇P
Molecular Weight:558.527
Hs Code.:

Synonyms:4-nitrophenylcarbonic acid 3-diphenylphosphanyl-4-propylcarbamoyloxybenzyl ester

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Chemical Property of 4-nitrophenylcarbonic acid 3-diphenylphosphanyl-4-propylcarbamoyloxybenzyl ester

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Technology Process of 4-nitrophenylcarbonic acid 3-diphenylphosphanyl-4-propylcarbamoyloxybenzyl ester

There total 5 articles about 4-nitrophenylcarbonic acid 3-diphenylphosphanyl-4-propylcarbamoyloxybenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 896740-41-3
propylcarbamic acid 2-diphenylphosphanyl-4-hydroxymethylphenyl ester

: 7693-46-1
4-Nitrophenyl chloroformate

: 896740-42-4
4-nitrophenylcarbonic acid 3-diphenylphosphanyl-4-propylcarbamoyloxybenzyl ester

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 3.5h; cooling;
DOI:10.1016/j.bmcl.2006.03.073

Reference yield:

: 60032-63-5
4-hydroxy-3-iodo-benzaldehyde

: 896740-42-4
4-nitrophenylcarbonic acid 3-diphenylphosphanyl-4-propylcarbamoyloxybenzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 44 percent / potassium acetate; Pd(OAc)2 / acetonitrile / 130 °C

2: 91 percent / pyridine / CH₂Cl₂ / 48 h / 20 °C

3: 85 percent / NABH₄ / CHCl₃; propan-2-ol / 0.5 h / 20 °C

4: 58 percent / pyridine / CH₂Cl₂ / 3.5 h / 20 °C / cooling

With pyridine; palladium diacetate; sodium tetrahydroborate; potassium acetate; In dichloromethane; chloroform; isopropyl alcohol; acetonitrile;
DOI:10.1016/j.bmcl.2006.03.073

Reference yield:

: 896740-39-9
3-diphenylphosphanyl-4-hydroxybenzaldehyde

: 896740-42-4
4-nitrophenylcarbonic acid 3-diphenylphosphanyl-4-propylcarbamoyloxybenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / pyridine / CH₂Cl₂ / 48 h / 20 °C

2: 85 percent / NABH₄ / CHCl₃; propan-2-ol / 0.5 h / 20 °C

3: 58 percent / pyridine / CH₂Cl₂ / 3.5 h / 20 °C / cooling

With pyridine; sodium tetrahydroborate; In dichloromethane; chloroform; isopropyl alcohol;
DOI:10.1016/j.bmcl.2006.03.073