3-Methoxy-1-(4-methoxyphenyl)-1H-isoindolium-trifluoromethansulfonat

Base Information

Chemical Name:3-Methoxy-1-(4-methoxyphenyl)-1H-isoindolium-trifluoromethansulfonat
CAS No.:83889-42-3
Molecular Formula:CHF₃O₃S*C₁₆H₁₅NO₂
Molecular Weight:403.379
Hs Code.:

Synonyms:3-Methoxy-1-(4-methoxyphenyl)-1H-isoindolium-trifluoromethansulfonat

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Chemical Property of 3-Methoxy-1-(4-methoxyphenyl)-1H-isoindolium-trifluoromethansulfonat

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Technology Process of 3-Methoxy-1-(4-methoxyphenyl)-1H-isoindolium-trifluoromethansulfonat

There total 6 articles about 3-Methoxy-1-(4-methoxyphenyl)-1H-isoindolium-trifluoromethansulfonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 37459-58-8
3-(4-Methoxyphenyl)-isoindolin-1-on

: 333-27-7
methyl trifluoromethanesulfonate

: 83889-42-3
3-Methoxy-1-(4-methoxyphenyl)-1H-isoindolium-trifluoromethansulfonat

Guidance literature:: In dichloromethane; for 24h; Ambient temperature;

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 83889-42-3
3-Methoxy-1-(4-methoxyphenyl)-1H-isoindolium-trifluoromethansulfonat

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / aq. ammonium chloride, magnesium / methanol / 4 h / Heating

2: 90 percent / thionyl chloride / CHCl₃ / 30 h / Ambient temperature

3: 47 percent / FeCl₃ / 1,2-dichloro-ethane / 41 h / Ambient temperature

4: 65 percent / CH₂Cl₂ / 24 h / Ambient temperature

With thionyl chloride; ammonium chloride; iron(III) chloride; magnesium; In methanol; dichloromethane; chloroform; 1,2-dichloro-ethane;

Reference yield:

: 30696-82-3
3-Chlor-isoindolin-1-on

: 83889-42-3
3-Methoxy-1-(4-methoxyphenyl)-1H-isoindolium-trifluoromethansulfonat

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / FeCl₃ / 1,2-dichloro-ethane / 41 h / Ambient temperature

2: 65 percent / CH₂Cl₂ / 24 h / Ambient temperature

With iron(III) chloride; In dichloromethane; 1,2-dichloro-ethane;