1-phenoxyethyl diphenethylphosphinothioselenoate

Base Information

Chemical Name:1-phenoxyethyl diphenethylphosphinothioselenoate
CAS No.:1443532-68-0
Molecular Formula:C₂₄H₂₇OPSSe
Molecular Weight:473.478
Hs Code.:

Synonyms:1-phenoxyethyl diphenethylphosphinothioselenoate

Suppliers and Price of 1-phenoxyethyl diphenethylphosphinothioselenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenoxyethyl diphenethylphosphinothioselenoate

Chemical Property:

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Technology Process of 1-phenoxyethyl diphenethylphosphinothioselenoate

There total 3 articles about 1-phenoxyethyl diphenethylphosphinothioselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 766-94-9
vinyl phenyl ether

: bis(2-phenylethyl)phosphane sulfide

: 1443532-68-0
1-phenoxyethyl diphenethylphosphinothioselenoate

: 1443532-69-1
1-phenoxyethyl diphenethylphosphinoselenothioate

Guidance literature:: With selenium; In 1,4-dioxane; at 100 ℃; for 0.666667h; Overall yield = 90 %; Overall yield = 426 mg; Mechanism; Inert atmosphere;
DOI:10.1016/j.tet.2013.05.038

Reference yield:

: 766-94-9
vinyl phenyl ether

: 1354722-42-1
C₁₆H₁₉PSSe

: 1443532-68-0
1-phenoxyethyl diphenethylphosphinothioselenoate

: 1443532-69-1
1-phenoxyethyl diphenethylphosphinoselenothioate

Guidance literature:: With selenium; In 1,4-dioxane; at 20 - 25 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.tet.2013.05.038

Reference yield:

: bis(2-phenylethyl)phosphane sulfide

: 1443532-68-0
1-phenoxyethyl diphenethylphosphinothioselenoate

: 1443532-69-1
1-phenoxyethyl diphenethylphosphinoselenothioate

Guidance literature:: Multi-step reaction with 2 steps

1: selenium / 1,4-dioxane / 100 °C / Inert atmosphere

2: selenium / 1,4-dioxane / 0.17 h / 20 - 25 °C / Inert atmosphere

With selenium; In 1,4-dioxane;
DOI:10.1016/j.tet.2013.05.038