8-bromo-N-phenyloctanamide

Base Information

Chemical Name:8-bromo-N-phenyloctanamide
CAS No.:792933-06-3
Molecular Formula:C₁₄H₂₀BrNO
Molecular Weight:298.223
Hs Code.:

Synonyms:8-bromo-N-phenyloctanamide

Suppliers and Price of 8-bromo-N-phenyloctanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-bromo-N-phenyloctanamide

Chemical Property:

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Technology Process of 8-bromo-N-phenyloctanamide

There total 3 articles about 8-bromo-N-phenyloctanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.6%

: 73674-09-6
8-bromo-n-octanoyl chloride

: 62-53-3
aniline

: 792933-06-3
8-bromo-N-phenyloctanamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 4h; Cooling with ice;
DOI:10.1007/s00044-011-9879-7

Reference yield:

: 123-99-9,26776-28-3
azelaic acid

: 792933-06-3
8-bromo-N-phenyloctanamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / toluene / 8 h / Reflux

2.1: sodium hydroxide / ethanol / 1 h / 20 °C

3.1: potassium hydroxide; silver nitrate / water / 0.33 h / 20 °C

3.2: 1.5 h / Cooling with ice

4.1: water; sodium hydroxide / 2 h / 45 °C

5.1: thionyl chloride / 1 h / Reflux

6.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Cooling with ice

With thionyl chloride; water; toluene-4-sulfonic acid; silver nitrate; triethylamine; potassium hydroxide; sodium hydroxide; In ethanol; dichloromethane; water; toluene;
DOI:10.1007/s00044-011-9879-7

Reference yield:

: 17696-11-6
8-bromooctanoic acid

: 792933-06-3
8-bromo-N-phenyloctanamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h

2: triethylamine / dichloromethane / 1 h

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;