phenylmethanol

Base Information

Chemical Name:phenylmethanol
CAS No.:75400-58-7
Molecular Formula:C₁₆H₁₉NO₃
Molecular Weight:273.332
Hs Code.:

<N-(tert-butoxycarbonyl)pyrrol-2-yl>phenylmethanol

Synonyms:phenylmethanol

Suppliers and Price of phenylmethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylmethanol

Chemical Property:

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Technology Process of phenylmethanol

There total 2 articles about phenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₉H₁₂LiNO₂

: 100-52-7
benzaldehyde

: 75400-58-7
phenylmethanol

Guidance literature:: at -80 ℃; for 2.3h;
DOI:10.1021/jo00314a034

Reference yield:

: 5176-27-2
N-tert-butyloxycarbonyl-pyrrole

: 75400-58-7
phenylmethanol

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium, 2,2,6,6-tetramethylpiperidine / tetrahydrofuran / 0.75 h / -80 °C

2: 75 percent / 2.3 h / -80 °C

With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; In tetrahydrofuran;
DOI:10.1021/jo00314a034