para-methoxyphenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

• Chemical Name: para-methoxyphenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
• CAS No.: 1205570-55-3
• Molecular Formula: C₆₀H₇₀O₂₄
• Molecular Weight: 1175.2

Synonyms:para-methoxyphenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Chemical Property of para-methoxyphenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of para-methoxyphenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 1 articles about para-methoxyphenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4-methoxyphenyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside (774591-92-3) + 4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2,3,6-tri-O-acetyl-α/β-D-glucopyranosyl trichloroacetimidate (250330-69-9) → para-methoxyphenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside (1205570-55-3)

Guidance literature:

4-methoxyphenyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside; 4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2,3,6-tri-O-acetyl-α/β-D-glucopyranosyl trichloroacetimidate; In dichloromethane; at 20 ℃; for 1h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 ℃; for 2h;

DOI:10.1021/ja1046523

Reference yield:

para-methoxyphenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-acetyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside (1205570-55-3) → C39H52O24

Guidance literature:

With hydrogen; palladium(II) hydroxide; In methanol; ethyl acetate; for 12h;

DOI:10.1021/ja1046523

upstream raw materials:

4-methoxyphenyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2,3,6-tri-O-acetyl-α/β-D-glucopyranosyl trichloroacetimidate

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