2,7,12-tris-[2-[4-formyl-2-allyloxyphenoxy]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-2H-tribenzo[a,d,g]cyclononene

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Chemical Name:2,7,12-tris-[2-[4-formyl-2-allyloxyphenoxy]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-2H-tribenzo[a,d,g]cyclononene
CAS No.:1268721-33-0
Molecular Formula:C₆₀H₆₀O₁₅
Molecular Weight:1021.13
Hs Code.:

Synonyms:2,7,12-tris-[2-[4-formyl-2-allyloxyphenoxy]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-2H-tribenzo[a,d,g]cyclononene

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Chemical Property of 2,7,12-tris-[2-[4-formyl-2-allyloxyphenoxy]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-2H-tribenzo[a,d,g]cyclononene

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Technology Process of 2,7,12-tris-[2-[4-formyl-2-allyloxyphenoxy]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-2H-tribenzo[a,d,g]cyclononene

There total 1 articles about 2,7,12-tris-[2-[4-formyl-2-allyloxyphenoxy]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-2H-tribenzo[a,d,g]cyclononene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 52507-49-0
4-hydroxy-3-(2-propenyloxy)benzaldehyde

: 188120-06-1
(±)-2,7,12-trimethoxy-3,8,13-tris(2-bromoethoxy)-10,15-dihydro-5H-tribenzo[a,d,g]cyclononene

: 1268721-33-0
2,7,12-tris-[2-[4-formyl-2-allyloxyphenoxy]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-2H-tribenzo[a,d,g]cyclononene

Guidance literature:: With caesium carbonate; In dimethyl sulfoxide; at 55 ℃; Inert atmosphere;
DOI:10.1021/ol200088f

Reference yield: 85.0%

: 1268721-33-0
2,7,12-tris-[2-[4-formyl-2-allyloxyphenoxy]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-2H-tribenzo[a,d,g]cyclononene

: 1268721-37-4
6,6',6''-((((3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g][9]annulene-2,7,12-triyl)tris-(oxy))tris(ethane-2,1-diyl))tris(oxy))tris(3-(hydroxymethyl)phenol)

Guidance literature:: 2,7,12-tris-[2-[4-formyl-2-allyloxyphenoxy]ethoxy]-3,8,13-trimethoxy-10,15-dihydro-2H-tribenzo[a,d,g]cyclononene; With sodium tetrahydroborate; In tetrahydrofuran; methanol; at -10 - 20 ℃; for 48h;

With hydrogenchloride; water;
DOI:10.1021/ol200088f