p-<(E)-2-(1,1,3,3-tetramethyl-5-indanyl)-propenyl>-benzoic acid ethylester

Base Information

Chemical Name:p-<(E)-2-(1,1,3,3-tetramethyl-5-indanyl)-propenyl>-benzoic acid ethylester
CAS No.:71441-07-1
Molecular Formula:C₂₅H₃₀O₂
Molecular Weight:362.512
Hs Code.:

Synonyms:p-<(E)-2-(1,1,3,3-tetramethyl-5-indanyl)-propenyl>-benzoic acid ethylester

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Chemical Property of p-<(E)-2-(1,1,3,3-tetramethyl-5-indanyl)-propenyl>-benzoic acid ethylester

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Technology Process of p-<(E)-2-(1,1,3,3-tetramethyl-5-indanyl)-propenyl>-benzoic acid ethylester

There total 7 articles about p-<(E)-2-(1,1,3,3-tetramethyl-5-indanyl)-propenyl>-benzoic acid ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.6%

: 6287-86-1
p-ethoxycarbonylbenzaldehyde

: 69251-31-6
<1-(1,1,3,3-tetramethyl-5-indanyl)ethyl>-triphenylphosphonium bromide

: 71441-07-1
p-<(E)-2-(1,1,3,3-tetramethyl-5-indanyl)-propenyl>-benzoic acid ethylester

Guidance literature:: With tetrahydrofuran; at 65 ℃; for 12h;

Reference yield:

: 17610-14-9
1-(1,1,3,3-tetramethyl-2,3-dihydro-1H-inden-5-yl)ethan-1-one

: 71441-07-1
p-<(E)-2-(1,1,3,3-tetramethyl-5-indanyl)-propenyl>-benzoic acid ethylester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium borohydride / methanol / 1.5 h / 0 °C

2: phosphorus tribromide / pyridine / diethyl ether; hexane / 2.5 h / 0 - 5 °C

3: diethyl ether; xylene / 48 h / 100 °C

4: 57.6 percent / butylene oxide / 12 h / 65 °C

With tetrahydrofuran; sodium tetrahydroborate; phosphorus tribromide; pyridine; In methanol; diethyl ether; hexane; xylene;

Reference yield:

: 69251-15-6
α-methyl-(1,1,3,3-tetramethyl-5-indane) methanol

: 71441-07-1
p-<(E)-2-(1,1,3,3-tetramethyl-5-indanyl)-propenyl>-benzoic acid ethylester

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus tribromide / pyridine / diethyl ether; hexane / 2.5 h / 0 - 5 °C

2: diethyl ether; xylene / 48 h / 100 °C

3: 57.6 percent / butylene oxide / 12 h / 65 °C

With tetrahydrofuran; phosphorus tribromide; pyridine; In diethyl ether; hexane; xylene;