ethyl 3-(2-cyclopropyl-4-(N'-hydroxycarbamimidoyl)phenyl)propanoate

Base Information

Chemical Name:ethyl 3-(2-cyclopropyl-4-(N'-hydroxycarbamimidoyl)phenyl)propanoate
CAS No.:1334481-26-3
Molecular Formula:C₁₅H₂₀N₂O₃
Molecular Weight:276.335
Hs Code.:

Synonyms:ethyl 3-(2-cyclopropyl-4-(N'-hydroxycarbamimidoyl)phenyl)propanoate

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Chemical Property of ethyl 3-(2-cyclopropyl-4-(N'-hydroxycarbamimidoyl)phenyl)propanoate

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Technology Process of ethyl 3-(2-cyclopropyl-4-(N'-hydroxycarbamimidoyl)phenyl)propanoate

There total 5 articles about ethyl 3-(2-cyclopropyl-4-(N'-hydroxycarbamimidoyl)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1334481-25-2
ethyl 3-(2-cyclopropyl-4-(N'-hydroxycarbamimidoyl)phenyl)acrylate

: 1334481-26-3
ethyl 3-(2-cyclopropyl-4-(N'-hydroxycarbamimidoyl)phenyl)propanoate

Guidance literature:: With hydrogen; sodium acetate; palladium dichloride; In methanol; for 5h;

Reference yield:

: 2315-86-8
3-bromo-4-hydroxybenzonitrile

: 1334481-26-3
ethyl 3-(2-cyclopropyl-4-(N'-hydroxycarbamimidoyl)phenyl)propanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: tricyclohexylphosphine; potassium phosphate / palladium diacetate / toluene; water / 100 °C / Inert atmosphere

2.1: pyridine / dichloromethane / 0.17 h / 0 °C

2.2: 2 h / 20 °C

3.1: triethylamine; (diphenylphosphin)ferrocene / palladium diacetate / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

4.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / methanol / 6 h / 75 °C

5.1: hydrogen; sodium acetate / palladium dichloride / methanol / 5 h

With pyridine; (diphenylphosphin)ferrocene; potassium phosphate; hydroxylamine hydrochloride; hydrogen; sodium acetate; sodium hydrogencarbonate; triethylamine; tricyclohexylphosphine; palladium diacetate; palladium dichloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 3.1: Heck Reaction;

Reference yield:

: 1334481-22-9
3-cyclopropyl-4-hydroxybenzonitrile

: 1334481-26-3
ethyl 3-(2-cyclopropyl-4-(N'-hydroxycarbamimidoyl)phenyl)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / dichloromethane / 0.17 h / 0 °C

1.2: 2 h / 20 °C

2.1: triethylamine; (diphenylphosphin)ferrocene / palladium diacetate / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

3.1: hydroxylamine hydrochloride; sodium hydrogencarbonate / methanol / 6 h / 75 °C

4.1: hydrogen; sodium acetate / palladium dichloride / methanol / 5 h

With pyridine; (diphenylphosphin)ferrocene; hydroxylamine hydrochloride; hydrogen; sodium acetate; sodium hydrogencarbonate; triethylamine; palladium diacetate; palladium dichloride; In methanol; dichloromethane; N,N-dimethyl-formamide; 2.1: Heck Reaction;