N-phenyl-1-(2'-methylphenyl)ethyl amine

Base Information

• Chemical Name: N-phenyl-1-(2'-methylphenyl)ethyl amine
• CAS No.: 731797-92-5
• Molecular Formula: C₁₅H₁₇N
• Molecular Weight: 211.307
• Mol file: 731797-92-5.mol

Synonyms:N-phenyl-1-(2'-methylphenyl)ethyl amine

Chemical Property of N-phenyl-1-(2'-methylphenyl)ethyl amine

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of N-phenyl-1-(2'-methylphenyl)ethyl amine

There total 5 articles about N-phenyl-1-(2'-methylphenyl)ethyl amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[1-(2'-methylphenyl)-ethylidene]-aniline (10228-83-8) → N-phenyl-1-(2'-methylphenyl)ethyl amine (731797-92-5,791808-29-2) + N-phenyl-1-(2'-methylphenyl)ethyl amine (791808-29-2)

Guidance literature:

With trichlorosilane; (S)-N-(3,5-dimethoxyphenyl)-2-[formyl(methyl)amino]-3-methylbutanamide; In toluene; at 20 ℃; for 16h; Title compound not separated from byproducts;

DOI:10.1021/ol049213+

Reference yield:

2-Methylacetophenone (577-16-2,122382-54-1) → N-phenyl-1-(2'-methylphenyl)ethyl amine (731797-92-5,791808-29-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 4 Angstroem molecular sieves / toluene / 12 h / 80 °C

2: Cl₃SiH; (2S)-2-[formyl(methyl)amino]-3-Me-N-(3,5-Me₂C₆H₃)butanamide / toluene / 16 h / 20 °C

With 4 A molecular sieve; trichlorosilane; (S)-N-(3,5-dimethoxyphenyl)-2-[formyl(methyl)amino]-3-methylbutanamide; In toluene;

DOI:10.1021/ol049213+

Reference yield:

aniline (62-53-3) → N-phenyl-1-(2'-methylphenyl)ethyl amine (731797-92-5,791808-29-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / toluene / Heating

2: PhSiH3; polymethylhydrosiloxane; isobutylamine / ethylenebis(η⁵-tetrahydroindenyl)titanium difluoride / methanol; toluene / 13 h / 60 °C

With polymethylhydrosiloxane; phenylsilane; isobutylamine; rac-(ethylene-1,2-bis(4,5,6,7-tetrahydro-1-indenyl))TiF₂; In methanol; toluene; 1: Substitution / 2: Reduction;

DOI:10.1021/ol005583w

upstream raw materials:

N-[1-(2'-methylphenyl)-ethylidene]-aniline

N-[1-(2'-methylphenyl)-ethylidene]-aniline

aniline

2-Methylacetophenone