(2,2,3,3,3-Pentafluoropropyl)benzene

Base Information

• Chemical Name: (2,2,3,3,3-Pentafluoropropyl)benzene
• CAS No.: 78693-66-0
• Molecular Formula: C₉H₇F₅
• Molecular Weight: 210.147
• Mol file: 78693-66-0.mol

Synonyms:2,2,3,3,3-pentafluoro-1-phenylpropane

Chemical Property of (2,2,3,3,3-Pentafluoropropyl)benzene

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

(2,2,3,3,3-Pentafluoropropyl)benzene 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2,2,3,3,3-Pentafluoropropyl)benzene

There total 10 articles about (2,2,3,3,3-Pentafluoropropyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

pentafluoroethylcopper(I) (60007-39-8) + benzyl bromide (100-39-0) → 2,2,3,3,3-pentafluoro-1-phenylpropane (78693-66-0)

Guidance literature:

With pyridine hydrogenfluoride; In diethyl ether; water; at 23 ℃; for 24h; Sealed tube;

DOI:10.1021/ja407017j

Reference yield: 73.0%

Toluene-4-sulfonic acid 2,2,3,3,3-pentafluoro-1-phenyl-propyl ester (78693-68-2) → 2,2,3,3,3-pentafluoro-1-phenylpropane (78693-66-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate;

DOI:10.1021/ja00408a024

Reference yield:

dibromodifluoromethane (75-61-6) + benzyl alcohol (100-51-6,185532-71-2) → benzyl fluoride (350-50-5) + (2,2,2-trifluoroethyl)benzene (21249-93-4) + 2,2,3,3,3-pentafluoro-1-phenylpropane (78693-66-0)

Guidance literature:

In N,N-dimethyl-formamide; at 100 ℃; Product distribution; Mechanism; var. amides as solvents, other aryl alcohols;

DOI:10.1016/S0022-1139(00)82418-5

upstream raw materials:

dibromodifluoromethane

benzyl bromide

metyhyl chlorodifluoroacetate

trimethyl(pentafluoroethyl)silane