Technology Process of C30H29N3O3
There total 3 articles about C30H29N3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
cyclohexa-1,4-diene; palladium 10% on activated carbon;
In
ethanol;
for 24h;
Reflux;
DOI:10.1016/j.bmcl.2012.11.011
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0) / toluene / 1 h / Reflux
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
3: lithium perchlorate / acetonitrile / 1 h / 20 °C
4: palladium 10% on activated carbon; cyclohexa-1,4-diene / ethanol / 24 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); cyclohexa-1,4-diene; palladium 10% on activated carbon; lithium perchlorate; 3-chloro-benzenecarboperoxoic acid;
In
ethanol; dichloromethane; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.11.011
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triphenylphosphine; 1,1,1,3,3,3-hexachloro-propan-2-one / dichloromethane / 0.58 h / -10 - 20 °C
2: tetrakis(triphenylphosphine) palladium(0) / toluene / 1 h / Reflux
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
4: lithium perchlorate / acetonitrile / 1 h / 20 °C
5: palladium 10% on activated carbon; cyclohexa-1,4-diene / ethanol / 24 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); 1,1,1,3,3,3-hexachloro-propan-2-one; cyclohexa-1,4-diene; palladium 10% on activated carbon; lithium perchlorate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine;
In
ethanol; dichloromethane; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.11.011
