C₁₂H₁₅NO₂

Base Information

Chemical Name:C₁₂H₁₅NO₂
CAS No.:1620074-30-7
Molecular Formula:C₁₂H₁₅NO₂
Molecular Weight:205.257
Hs Code.:

C<sub>12</sub>H<sub>15</sub>NO<sub>2</sub>

Synonyms:C₁₂H₁₅NO₂

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Chemical Property of C₁₂H₁₅NO₂

Chemical Property:

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Technology Process of C₁₂H₁₅NO₂

There total 6 articles about C₁₂H₁₅NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1013-88-3
Benzophenone imine

: 1620074-29-4
C₁₂H₁₃BrO₂

: 1620074-30-7
C₁₂H₁₅NO₂

Guidance literature:: With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 110 ℃; for 18h; Inert atmosphere;

Reference yield:

: 638220-35-6
1-(4-bromophenyl)-cyclopropanecarboxylic acid methyl ester

: 1620074-30-7
C₁₂H₁₅NO₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -4 °C

2.1: triethylamine / dichloromethane / 3 h / -78 - 0 °C

3.1: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C

4.1: sodium hydroxide / methanol; water / 16 h / 60 °C

4.2: pH 3

5.1: hydrogenchloride / 18 h / Reflux

6.1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 18 h / 110 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 98480-31-0
(1-(4-bromophenyl)cyclopropyl)methanol

: 1620074-30-7
C₁₂H₁₅NO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 3 h / -78 - 0 °C

2.1: triethylamine / N,N-dimethyl-formamide / 3 h / 70 °C

3.1: sodium hydroxide / methanol; water / 16 h / 60 °C

3.2: pH 3

4.1: hydrogenchloride / 18 h / Reflux

5.1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 18 h / 110 °C / Inert atmosphere

With hydrogenchloride; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; sodium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;