N6-benzoyl-2'-deoxy-α-C-(1-phenylethane-1,2-diol)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)adenosine

Base Information

Chemical Name:N6-benzoyl-2'-deoxy-α-C-(1-phenylethane-1,2-diol)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)adenosine
CAS No.:1276113-10-0
Molecular Formula:C₃₇H₅₁N₅O₇Si₂
Molecular Weight:734.012
Hs Code.:

Synonyms:N6-benzoyl-2'-deoxy-α-C-(1-phenylethane-1,2-diol)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)adenosine

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Chemical Property of N6-benzoyl-2'-deoxy-α-C-(1-phenylethane-1,2-diol)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)adenosine

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Technology Process of N6-benzoyl-2'-deoxy-α-C-(1-phenylethane-1,2-diol)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)adenosine

There total 7 articles about N6-benzoyl-2'-deoxy-α-C-(1-phenylethane-1,2-diol)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18043-71-5
1,1,3,3-tetraisopropyldisiloxane

: 1276113-10-0
N6-benzoyl-2'-deoxy-α-C-(1-phenylethane-1,2-diol)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)adenosine

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 3 h / 20 °C

2: dmap / acetonitrile / 20 °C

3: 2,2'-azobis(isobutyronitrile) / benzene / 50 h / 40 - 80 °C

4: pyridine / 5 h / 20 °C

5: osmium(VIII) oxide; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 24 h / 0 - 4 °C

With pyridine; dmap; osmium(VIII) oxide; 2,2'-azobis(isobutyronitrile); potassium carbonate; potassium hexacyanoferrate(III); In water; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1002/ejoc.201001448

Reference yield:

: C₃₇H₄₉N₅O₅Si₂

: 1276113-10-0
N6-benzoyl-2'-deoxy-α-C-(1-phenylethane-1,2-diol)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)adenosine

Guidance literature:: With osmium(VIII) oxide; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 - 4 ℃; for 24h;
DOI:10.1002/ejoc.201001448

Reference yield:

: 2'-deoxy-2'-α-C-styryl-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)adenosine

: 1276113-10-0
N6-benzoyl-2'-deoxy-α-C-(1-phenylethane-1,2-diol)-3',5'-O-(1,1,3,3-tetraisopropyldisiloxan-1,3-diyl)adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 5 h / 20 °C

2: osmium(VIII) oxide; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 24 h / 0 - 4 °C

With pyridine; osmium(VIII) oxide; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol;
DOI:10.1002/ejoc.201001448