4-benzoyl-3-carboxamido-1-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-1,4-dihydropyridine

Base Information

Chemical Name:4-benzoyl-3-carboxamido-1-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-1,4-dihydropyridine
CAS No.:872216-65-4
Molecular Formula:C₂₄H₂₆N₂O₉
Molecular Weight:486.478
Hs Code.:

Synonyms:4-benzoyl-3-carboxamido-1-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-1,4-dihydropyridine

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Chemical Property of 4-benzoyl-3-carboxamido-1-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-1,4-dihydropyridine

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Technology Process of 4-benzoyl-3-carboxamido-1-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-1,4-dihydropyridine

There total 7 articles about 4-benzoyl-3-carboxamido-1-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-1,4-dihydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (2S,3S,4S,5S)-4-acetoxy-5-acetoxymethyl-2-((1R,7aR)-1-hydroxy-3-oxo-1-phenyl-1,2,3,7a-tetrahydro-pyrrolo[3,4-c]pyridin-5-yl)-tetrahydro-furan-3-yl ester

: 872216-65-4
4-benzoyl-3-carboxamido-1-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-1,4-dihydropyridine

Guidance literature:: In methanol; dichloromethane; ethyl acetate; at 20 ℃;
DOI:10.1021/jo051901z

Reference yield:

: 849322-40-3
1-hydroxy-1-phenyl-1,2-dihydro-3H-pyrrolo[3,4-c]pyridin-3-one

: 872216-65-4
4-benzoyl-3-carboxamido-1-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / acetonitrile / 4 h / 20 °C

2: NaBH(Ac)3; acetic acid / ethanol / 0.17 h / 0 °C

3: CH₂Cl₂; methanol; ethyl acetate / 20 °C

With sodium tris(acetoxy)borohydride; acetic acid; In methanol; ethanol; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/jo051901z

Reference yield:

: 5-(3,4-diacetoxy-5-acetoxymethyl-tetrahydro-furan-2-yl)-1-hydroxy-3-oxo-1-phenyl-2,3-dihydro-1H-pyrrolo[3,4-c]pyridin-5-ium; bromide

: 872216-65-4
4-benzoyl-3-carboxamido-1-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH(Ac)3; acetic acid / ethanol / 0.17 h / 0 °C

2: CH₂Cl₂; methanol; ethyl acetate / 20 °C

With sodium tris(acetoxy)borohydride; acetic acid; In methanol; ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jo051901z