3,4-Pyridinedicarboximide

Base Information

• Chemical Name: 3,4-Pyridinedicarboximide
• CAS No.: 4664-01-1
• Molecular Formula: C7H4 N2 O2
• Molecular Weight: 148.121
• Hs Code.: 29333990
• European Community (EC) Number: 628-277-9
• NSC Number: 524479
• UNII: X0F2A90A07
• DSSTox Substance ID: DTXSID00196891
• Nikkaji Number: J14.602A
• Wikidata: Q72503885
• Mol file: 4664-01-1.mol

Synonyms:3,4-Pyridinedicarboximide;4664-01-1;Cinchomeronimide;3,4-Pyridinecarboximide;1H-Pyrrolo[3,4-c]pyridine-1,3(2H)-dione;Pyrrolo[3,4-c]pyridine-1,3-dione;2H-pyrrolo[3,4-c]pyridine-1,3-dione;Cinchomeronic acid imide;4-Azaphthalimid;Pyridine-3,4-dicarboximide;1H-Pyrrolo(3,4-c)pyridine-1,3(2H)-dione;1H,2H,3H-pyrrolo[3,4-c]pyridine-1,3-dione;MFCD00013439;4-Azaphthalimid [German];X0F2A90A07;NSC 524479;NSC-524479;BRN 0124195;PYRROLO(3,4-C)PYRIDINE-1,3-DIONE;SCHEMBL31318;UNII-X0F2A90A07;1H-Pyrrolo[3,3(2H)-dione;3,4-PYRIDINECARBOXYIMIDE;DTXSID00196891;3,4-Pyridinedicarboximide, 97%;NSC524479;RB1080;AKOS009157142;PS-4641;AC-23152;SY004813;LS-131169;AM20051209;CS-0010098;FT-0614409;EN300-76991;A918750;AC-907/25014351;J-507044;J-511230;Q-101245;F2167-7123;Z1123701770

Chemical Property of 3,4-Pyridinedicarboximide

Chemical Property:

• Melting Point: 232-235 °C(lit.)
• Refractive Index: 1.5300 (estimate)
• Boiling Point: °Cat760mmHg
• PKA: 7.80±0.20(Predicted)
• Flash Point: °C
• PSA: 59.06000
• Density: 1.469g/cm³
• LogP: 0.29400
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• XLogP3: -0.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 148.027277375
• Heavy Atom Count: 11
• Complexity: 215

Purity/Quality:

97% ^*data from raw suppliers

Pyridine-3,4-dicarboximide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CN=CC2=C1C(=O)NC2=O

Technology Process of 3,4-Pyridinedicarboximide

There total 3 articles about 3,4-Pyridinedicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-Lutidin (583-58-4) → 3-methyl-4-cyanopyridine (7584-05-6) + 3,4-pyridinedicarboximide (4664-01-1)

Guidance literature:

With (V₂O₅)(SnO₂)2; ammonia; water; oxygen; Temperature; Reagent/catalyst; Concentration; Catalytic behavior;

DOI:10.1134/S1070363212120146

Reference yield:

cinchomeronic anhydride (4664-08-8) → 3,4-pyridinedicarboximide (4664-01-1)

Guidance literature:

With urea; at 150 - 160 ℃; for 0.333333h; Yield given;

Reference yield:

acetamide (60-35-5) + cinchomeronic anhydride (4664-08-8) → 3,4-pyridinedicarboximide (4664-01-1)

Guidance literature:

DOI:10.1021/jo01153a015

upstream raw materials:

acetamide

cinchomeronic anhydride

3,4-Lutidin

Downstream raw materials:

2-hydroxyethylcinchomeronic imide

N-(dibenzylaminomethyl)pyridine-3,4-dicarboximide

3-Aminopyridine-4-carboxylic acid

ethyl 3-aminopyridine-4-carboxylate