C₂₉H₃₆FN₆O₉P

Base Information

Chemical Name:C₂₉H₃₆FN₆O₉P
CAS No.:1613592-01-0
Molecular Formula:C₂₉H₃₆FN₆O₉P
Molecular Weight:662.612
Hs Code.:

C<sub>29</sub>H<sub>36</sub>FN<sub>6</sub>O<sub>9</sub>P

Synonyms:C₂₉H₃₆FN₆O₉P

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Chemical Property of C₂₉H₃₆FN₆O₉P

Chemical Property:

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Technology Process of C₂₉H₃₆FN₆O₉P

There total 16 articles about C₂₉H₃₆FN₆O₉P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613589-53-9
C₄₉H₅₂FN₆O₁₀P

: 1613592-01-0
C₂₉H₃₆FN₆O₉P

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; acetonitrile; at 0 - 20 ℃; for 1h;

Reference yield:

: 10310-21-1
2-amino-6-chloropurine

: 1613592-01-0
C₂₉H₃₆FN₆O₉P

Guidance literature:: Multi-step reaction with 15 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; trimethylsilyl trifluoromethanesulfonate / acetonitrile; toluene / 0 - 70 °C

2: silver nitrate / dichloromethane / 20 °C / Inert atmosphere

3: sodium ethanolate / 20 °C

4: pyridine / 16 h / 0 °C

5: sodium iodide / acetone / Reflux

6: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 60 °C

7: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 20 °C / Cooling with ice

8: dmap / dichloromethane / 0 - 20 °C

9: 15-crown-5 / N,N-dimethyl-formamide / 48 h / 90 - 100 °C

10: ammonia / methanol / 18 h / 20 °C

11: 1H-imidazole; pyridine / 15 h / 0 - 20 °C

12: silver nitrate / dichloromethane / 20 °C / Inert atmosphere

13: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C

14: 1-methyl-1H-imidazole / acetonitrile / 2.5 h / 0 - 20 °C

15: hydrogenchloride / 1,4-dioxane; acetonitrile / 1 h / 0 - 20 °C

With pyridine; 1H-imidazole; 1-methyl-1H-imidazole; hydrogenchloride; dmap; N-iodo-succinimide; 15-crown-5; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; ammonia; sodium ethanolate; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); sodium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; acetonitrile;

Reference yield:

: 1613589-40-4
C₃₄H₃₃N₅O₆

: 1613592-01-0
C₂₉H₃₆FN₆O₉P

Guidance literature:: Multi-step reaction with 12 steps

1: pyridine / 16 h / 0 °C

2: sodium iodide / acetone / Reflux

3: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 60 °C

4: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 20 °C / Cooling with ice

5: dmap / dichloromethane / 0 - 20 °C

6: 15-crown-5 / N,N-dimethyl-formamide / 48 h / 90 - 100 °C

7: ammonia / methanol / 18 h / 20 °C

8: 1H-imidazole; pyridine / 15 h / 0 - 20 °C

9: silver nitrate / dichloromethane / 20 °C / Inert atmosphere

10: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C

11: 1-methyl-1H-imidazole / acetonitrile / 2.5 h / 0 - 20 °C

12: hydrogenchloride / 1,4-dioxane; acetonitrile / 1 h / 0 - 20 °C

With pyridine; 1H-imidazole; 1-methyl-1H-imidazole; hydrogenchloride; dmap; N-iodo-succinimide; 15-crown-5; tetrabutyl ammonium fluoride; ammonia; silver nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); sodium iodide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;