1,1-dimethylethyl [3-({4-bromo-5-[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-2-thienyl}amino)-3-oxo-2-phenylpropyl]carbamate

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Chemical Name:1,1-dimethylethyl [3-({4-bromo-5-[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-2-thienyl}amino)-3-oxo-2-phenylpropyl]carbamate
CAS No.:943321-95-7
Molecular Formula:C₃₁H₂₉BrN₄O₅S₂
Molecular Weight:681.631
Hs Code.:

Synonyms:1,1-dimethylethyl [3-({4-bromo-5-[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-2-thienyl}amino)-3-oxo-2-phenylpropyl]carbamate

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Chemical Property of 1,1-dimethylethyl [3-({4-bromo-5-[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-2-thienyl}amino)-3-oxo-2-phenylpropyl]carbamate

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Technology Process of 1,1-dimethylethyl [3-({4-bromo-5-[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-2-thienyl}amino)-3-oxo-2-phenylpropyl]carbamate

There total 2 articles about 1,1-dimethylethyl [3-({4-bromo-5-[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-2-thienyl}amino)-3-oxo-2-phenylpropyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26250-90-8,189619-55-4,262301-38-2
(3R)-benzyl-3-(tert-butoxycarbonyl)amino-propanoic acid

: C₁₆H₁₆BrN₃O₂S

: 943321-95-7
1,1-dimethylethyl [3-({4-bromo-5-[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-2-thienyl}amino)-3-oxo-2-phenylpropyl]carbamate

Guidance literature:: C₁₆H₁₆BrN₃O₂S; With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; for 0.25h;

(3R)-benzyl-3-(tert-butoxycarbonyl)amino-propanoic acid; In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 942919-24-6
1-(phenylsulfonyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo-[2,3-b]pyridine

: 1159682-82-2
C₁₈H₂₀Br₂N₂O₃S

: 943321-95-7
1,1-dimethylethyl [3-({4-bromo-5-[1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-yl]-2-thienyl}amino)-3-oxo-2-phenylpropyl]carbamate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; water; at 70 ℃;
DOI:10.1016/j.bmcl.2009.02.094