3-methoxyphenyl 3-thienyl sulfide

Base Information Edit

Chemical Name:3-methoxyphenyl 3-thienyl sulfide
CAS No.:128348-23-2
Molecular Formula:C₁₁H₁₀OS₂
Molecular Weight:222.332
Hs Code.:
Mol file:128348-23-2.mol

Synonyms:3-methoxyphenyl 3-thienyl sulfide

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Chemical Property of 3-methoxyphenyl 3-thienyl sulfide Edit

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Technology Process of 3-methoxyphenyl 3-thienyl sulfide

There total 2 articles about 3-methoxyphenyl 3-thienyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 872-31-1
3-Bromothiophene

: 15570-12-4
3-methoxybenzenethiol

: 128348-23-2
3-methoxyphenyl 3-thienyl sulfide

Guidance literature:: With copper; potassium carbonate; In N,N-dimethyl-formamide; for 13h; Heating;

Reference yield:

: 872-31-1
3-Bromothiophene

: 59014-89-0
bis(3-methoxyphenyl)disulfide

: 128348-23-2
3-methoxyphenyl 3-thienyl sulfide

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) ether, hexane, -78 deg C, 45 min. 2.) ether, -70 deg C to r.t., 16 h;
DOI:10.1002/jhet.5570270202